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GCMS analysis results, sample AE07627, April 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE07627 conducted April 9, 2002, detecting unknown compounds and 2,4-DDD surrogate at 94% recovery.

NYC-WTC_000047236–000047244

Folder label: “GCMS X 4/2/02 A 4/3/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020403\07627.D Vial: 18 Acq On 4 Apr 2002 12:48 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 04 08:15:06 2002 Quant Results File: SCAN020403.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Thu Apr 04 08:10:12 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 10.66 152 2647252 20.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 9673077 20.00 ug/1 0.00 17) Acenaphthene-dlO 23.66 164 5540699 20.00 ug/1 -0.01 31) Phenanthrene-diO 30.89 188 9091582 20.00 ug/1 0.00 39) Chrysene-dl2 39.09 240 6841793 20.00 ug/1 -0.02 45) Perylene-dl2 42.30 264 3554877 20.00 ug/1 -0.01 System Monitoring Compounds 2 8) TCMX 26.73 207 202743 3.74 ug/1 0.00 Spiked Amount 5>000 Recovery % = 74. 1-0 Target Compounds 19 Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 07627.D SCAN020403.M Thu Apr 04 10:45:51 2002 Page 1

NYC-WTC_000047238

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NYC-WTC_000047238Source: NYC Law Department, mirrored locally

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