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GCMS analysis report, sample AE07568, April 2002

Machine-extracted title · confidence 100%

Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.314 18 40 50 PV 3 10996 394584 1.65% 0.315% 2 3.385 50 52 55 W 3 3653 58891 0.25% 0.047% 3 3.420 55 58 65 W 4 4117 115245 0.48% 0.092% 4 5.047 327 335 338 W 2 2116 44342 0.18% 0.035% 5 5.588 417 427 438 PV 3 7442 195338 0.81% 0.156%

6 10.659 1279 1290 1314 PV 550008 14598068 60.89% 11.642% 7 14.689 1963 1976 1989 W 138446 3528208 14.72% 2.814% 8 15.770 2142 2160 2170 PV 784515 19230453 80.21% 15.336% 9 23.655 3486 3502 3518 PV 879074 22770228 94.98% 18.159% 10 26.722 4014 4024 4033 W 2 66939 1494926 6.24% . 1.192%

11 30.260 4620 4626 4641 W 2 2247 64085 0.27% 0.051% 12 30.894 4720 4734 4753 W 2 856033 23974721 100.00% 19.119% 13 31.129 4767 4774 4783 PV 2356 61124 0.25% 0.049% 14 39.096 6120 6130 6145 PV 2 1216878 21949145 91.55% 17.504% 15 41.253 6491 6497 6502 PV 3937 69128 0.29% 0.055%

16 42.163 6645 6652 6660 W 7971 178961 0.75% 0.143% 17 42.305 6665 6676 6701 W 2 789370 14657052 61.14% 11.689% 18 43.010 6787 6796 6810 W 3 12907 369332 1.54% 0.295% 19 43.174 6817 6824 6828 W 3 2646 67154 0.28% 0.054% 20 43.268 6828 6840 6841 W 3 3883 137446 0.57% 0.110%

21 43.292 6841 6844 6850 W 3 4361 112683 0.47% 0.090% 22 43.333 6850 6851 6859 W 4 3829 120278 0.50% 0.096% 23 43.392 6859 6861 6863 W 4402 53619 0.22% 0.043% 24 43.444. 6863 6870 6873 W 4 4650 144990 0.60% 0.116% 25 43.474 6873 6875 6881 W 3 5016 139126 0.58% 0.111%

26 43.533 6881 6885 6886 W 4 4790 79954 0.33% 0.064% 27 43.832 6922 6936 6946 W 2 13827 487105 2.03% 0.388% 28 44.778 7087 7097 7117 W 3 8550 299198 1.25% 0.239%

Sum of corrected areas: 125395385

07568.D SCAN020403.M Thu Apr 04 10:30:28 2002 Page 1

NYC-WTC_000047199

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