GCMS reference analysis results for sample AE07486, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR18O2\REFC1.D Vial: 15 Acq On : 20 Apr 2002 7:14 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 12:15 2002 Quant Results File: GCMS0419.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 442957 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1606698 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 926151 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1361268 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 883866 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 549378 20.00 ug/1 -0.05 System Monitoring Compounds 28) TCMX 23.28 209 33030 4.28 ug/L -0.05 Spiked Amount 4.000 Recovery = 107.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.86 74 89077 9.24 ug/1 99 3) bis(2-Chloroethyl)ether 11.61 93 215235 14.34 ug/1 98 4) 1,3-Dichlorobenzene 12.11 146 179356 11.59 ug/1 99 5) 1,4-Dichlorobenzene 12.25 146 189709 12.18 ug/1 100 6) 1,2-Dichlorobenzene 12.77 146 185787 12.85 ug/1 98 7) 2,21-oxybis(1-Chloropropan 13.09 45 289754 13.98 ug/1 99 8) N-Nitroso-di-n-propylamine 13.48 70 141032 14.33 ug/1 98 9) Hexachloroethane 13.62 117 53797 9.43 ug/1 89 11) Nitrobenzene 13.89 77 190779 13.54 ug/1 99 12) Isophorone 14.54 82 349097 13.10 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 . 261476 15.06 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 166684 13.65 ug/1 99 15) Naphthalene 15.90 128 571632 14.80 ug/1 99 16) Hexachlorobutadiene 16.45 225 63014 10.32 ug/1 99 18) Hexachlorocyclopentadiene 18.64 237 10367 2.53 ug/1 # 95 19) 2-Chloronaphthalene 19.41 162 352606 14.44 ug/1 97 20) Dimethylphthalate 20.49 163 486443 17.27 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 96207 14.29 ug/1 99 22) Acenaphthylene 20.67 152 531218 15.55 ug/1 99 23) Acenaphthene 21.24 153 378301 15.57 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 123062 13.89 ug/1 99 25) Diethylphthalate 22.63 149 457940 16.95 ug/1 98 26) 4-Chlorophenyl-phenylether 22.78 204 202747 16.92 ug/1 96 27) Fluorene 22.76 166 421946 16.40 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 385470 13.49 ug/L 97 31) N-Nitrosodiphenylamine 23.17 168 146638 12.95 ug/1 100 32) 4-Bromophenyl-phenylether 24.24 248 112129 16.97 ug/1 96 (#) = qualifier out of range (m) = manual integration REFC1.D GCMS0419.M Mon Apr 22 12:17:31 2002 Page 1

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