GCMS results for sample AE07416, Apr 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\041902\REFA0419.D Vial: 6 Acq On : 19 Apr 2002 4:41 pm Operator: Bohlk Sample : REFI 3/29/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 26 09:25:42 2002 Quant Results File: 5080402BBC.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Fri Apr 26 09:23:30 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.41 152 426769 40.00 ug/L 0.00 10) Naphthalene-d8 12.89 136 1833083 40.00 ug/L 0.00 17) Acenaphthene-diO 17.99 164 1029586 40.00 ug/L 0.00 30) Phenanthrene-diO 22.34 188 1416068 40.00 ug/L 0.00 39) Chrysene-dl2 30.15 240 1136002 40.00 ug/L 0.00 45) Perylene-dl2 34.02 264 681967 40.00 ug/L 0.00

System Monitoring Compounds 28) TCMX (SURR) 19.96 244 26367 6.42 ug/L 0.00 Spiked Amount 5.000 Recovery = 128.40% 38) 2,4-DDD (SURR) 0.00 235 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.51 74 109213m 8.85 ug/L 3) bis(2-chloroethyl) ether 8.86 93 242823 13.42 ug/L 82 4) 1,3 - Dichlorobenze 9.25 146 225616 15.26 ug/L 97 5) 1,4 - Dichlorobenzene 9.45 146 230102 14.54 ug/L 98 6) 1,2 - Dichlorobenzene 9.83 146 188123 14.54 ug/L 98 7) 2,2 1 - oxybis (l-Chloropr 10.30 45 485686 17.99 ug/L 93 8) N-Nitroso-di-n-propylamine 10.62 70 192414 14.92 ug/L 93 9) Hexachloroethane 10.72 117 102622 14.58 ug/L 97 11) Nitrobenzene 10.97 77 211649 11.90 ug/L 96 12) Isophorone 11.68 82 553843 15.65 ug/L 99 13) bis(2-Chloroethoxy) methan 12.43 93 297967 13.80 ug/L 99 14) 1,2,4-Trichlorobenzene 12.77 180 185804 15.67 ug/L 99 15) Naphthalene 12.94 128 829007 18.49 ug/L 98 16) Hexachlorobutadiene 13.40 225 99980 17.49 ug/L 98 18) Hexachlorocyclopentadiene 15.48 237 15980 3.32 ug/L 91 19) 2-chloronaphthalene 16.37 162 370632 17.80 ug/L 97 20) Dimethylphthalate 17.46 163 553815 18.70 ug/L 97 21) 2,6-Dinitrotoluene 17.56 165 83387 14.46 ug/L 95 22) Acenaphthylene 17.55 152 582989 15.31 ug/L 99 23) Acenaphthene 18.08 153 473794 19.67 ug/L 97 24) 2,4-Dinitrotoluene 18.72 165 74185 10.68 ug/L 97 25) Diethylphthalate 19.58 149 547587 22.27 ug/L 98 26) 4-Chlorophenyl-phenyl ethe 19.75 204 251905 18.53 ug/L 100 27) Fluorene 19.61 166 573042 20.62 ug/L 97 29) Azobenzen/ 1,2-Diphenylhyd 20.20 77 735061 17.19 ug/L 95 31) N-Nitrosodiphenylamine 20.12 169 264017 17.49 ug/L 97 32) 4-Bromophenyl-phenyl ether 21.17 248 119278 18.20 ug/L 89 33) Hexachlorobenzene 21.19 284 122737 20.04 ug/L 86 34) Phenanthrene 22.40 178 803898 20.49 ug/L 99 35) Anthracene 22.55 178 667708 16.68 ug/L 98 36) Di-n-butylphthalate 24.51 149 997977 22.24 ug/L 98 37) Fluoranthene 25.90 202 767146 18.43 ug/L 84 40) Pyrene 26.53 202 886665 20.70 ug/L 89 41) Butylbenzylphthalate 28.90 149 334800 16.92 ug/L 86 42) Benzo (a) antracene 30.13 228 596174 17.23 ug/L 99 43) Bis (2-ethylhexyl) phthala 30.77 149 503099 17.90 ug/L 97 44) Chrysene 30.22 228 670239 19.57 ug/L 99

(#) = qualifier out of range (m) = manual integration REFA0419.D 5080402BBC.M Fri Apr 26 09:26:52 2002 Page 1

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