GCMS reference standard results for sample AE07416, Apr 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

• Data File C:\MSDCHEM\1\DATA\041902\C8040419.D Vial: 2 Acq On 19 Apr 2002 1:10 pm 5 Operator: Bohik Sample C80 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 19 14:08:42 2002 Quant Results File: 5080402BBC.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Tue Apr 16 18:27:45 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.42 152 469724 40.00 ug/L 0.00 10) Naphthalene-d8 12.90 136 1984267 40.00 ug/L 0.01 17) Acenaphthene-diO 18.00 164 1077172 40.00 ug/L 0.01 30) Phenanthrene-dlO 22.35 188 1552126 40.00 ug/L 0.01 39) Chrysene-dl2 30.18 240 1163798 40.00 ug/L 0.03 45) Perylene-dl2 34.03 264 734844 40.00 ug/L 0.02

System Monitoring Compounds 28) TCMX (SURR) 19.97 244 44478 10.35 ug/L 0.01 Spiked Amount 10.000 Recovery = 103.50% 38) 2,4-DDD (SURR) 0.00 235 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% ((2 Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.45 74 2225009 163.80 ug/L 85 3) bis(2-chloroethyl) ether 8.86 93 3343763 167.89 ug/L 82 4) 1,3 - Dichlorobenze 9.25 146 2575711 158.28 ug/L 100 5) 1,4 - Dichlorobenzene 9.47 146 2739060 157.24 ug/L 98 6) 1,2 - Dichlorobenzene 9.84 146 2362209 165.91 ug/L 98 7) 2,2 1 - oxybis (l-Chloropr 10.31 45 4697340 158.10 ug/L 95 8) N-Nitroso-di-n-propylamine 10.66 70 2338619 164.73 ug/L 93 9) Hexachloroethane 10.73 117 1174252 151.57 ug/L 98 11) Nitrobenzene 11.00 77 3335603 173.23 ug/L 99 12) Isophorone 11.70 82 6053670 158.03 ug/L 98 13) bis(2-Chloroethoxy) methan 12.46 93 3745887 160.29 ug/L 100 14) 1,2,4-Trichlorobenzene 12.78 180 1962707 152.89 ug/L 99 15) Naphthalene 12.97 128 7106001 146.45 ug/L 99 16) Hexachlorobutadiene 13.40 225 971474 157.00 ug/L 99 18) Hexachlorocyclopentadiene 15.48 237 965204 191.47 ug/L 98 19) 2-chloronaphthalene 16.39 162 3680414 168.90 ug/L 98 20) Dimethylphthalate 17.50 163 4983132 160.85 ug/L 99 21) 2,6-Dinitrotoluene 17.62 165 1045280 173.21 ug/L 99 22) Acenaphthylene 17.57 152 6437347 161.59 ug/L 99 23) Acenaphthene 18.11 153 3730525 148.05 ug/L 99 24) 2,4-Dinitrotoluene 18.76 165 1270308 174.76 ug/L 99 25) Diethylphthalate 19.62 149 3792146 147.43 ug/L 98 26) 4-Chlorophenyl-phenyl ethe 19.78 204 2167198 152.39 ug/L 98 27) Fluorene 19.64 166 4245358 146.05 ug/L 100 29) Azobenzen/ 1,2-Diphenylhyd 20.23 77 6779960 151.57 ug/L 97 31) N-Nitrosodiphenylamine 20.15 169 2490210 150.48 ug/L 99 32) 4-Bromophenyl-phenyl ether 21.19 248 1131155 157.50 ug/L 94 33) Hexachlorobenzene 21.23 284 1048181 156.14 ug/L 98 34) Phenanthrene 22.44 178 6422832 149.33 ug/L 98 35) Anthracene 22.59 178 6692800 152.54 ug/L 100 36) Di-n-butylphthalate 24.53 149 7602151 154.56 ug/L 99 37) Fluoranthene 25.94 202 7433709 162.96 ug/L 94 40) Pyrene 26.57 202 7091155 161.57 ug/L 96 41) Butylbenzylphthalate 28.93 149 3451502 170.24 ug/L 92 42) Benzo (a) antracene 30.16 228 5914386 166.86 ug/L 99 43) Bis (2-ethylhexyl) phthala 30.79 149 4632882 160.90 ug/L 98 44) Chrysene 30.27 228 5688006 162.12 ug/L 99

(#) = qualifier out of range (m) = manual integration C80A0419.D 5080402BBC.M Fri Apr 19 14:09:23 2002 Page 1

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