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GCMS results for sample AE08068, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08068 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046813–000046840

Folder label: “GCMS X 4/5/02 A 4/16/02

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Scanned page image, NYC-WTC_000046824
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 2-Hexanone Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

4.87 0.43 ug/L 283291 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 86 2 2-Hexanone 100 C6H120 000591-78-6 86 3 Oxirane, 2-methyl-2-(1-methyleth... 100 C6H120 072221-03-5 72 4 2-Hexanone 100 C6H120 000591-78-6 64 Abundance Scan 305 (4 871 min) 08068 D (-300) (-) m/z 43.30 100.00% 43 58 5000

100

n/z-> 0+ _r,.......,,,,^.,.,1/11 10 20 30 40 +51 50 60 j________ L 71 I ' ' ' ' I ' 70 80 85 ,1, 90 100 TT m/z 4 60 4 80 58.30 5 00 5 20 66.18% Abundance #5779 2-Hexanone 43

5000 58 . ... , YYM A, A . . 4.60 4 80 5.00 5 20 29 m/z 41.25 19.31%

n/z-> 0+ IIP 10 15 20 11111738,1 30 40 +r 50 53 1 ri-' it. 71. 60 70 80 90 100 Abundance #109711: 2-Hexanone 43 ■) ... r 1 I T 1 Ti i Di"1 1 4.60 4 80 5 00 5.20 58 5000 m/ z 57.30) 15.80%

29 85 100 01 ■ i ' ■ • ' i 134 48 53 I , 65.71 ' 80' ' . 909...100 I tr ■ r' ■ 1...... 77 n/z- > Abundance 10 20 30 40 50 60 70 #5754 Oxirane, 2-methyl-2-(1-methylethyl)- 43 P 4 60 4.80 AM. 5.00 5.20 58 m/z 100.30 13.40% 5000 29 71 85 100

n/z-> 0 .... .. 39 10 20 30 40 — 50 52 66 I'!-- .-I ■ ,1, , 60 70 80 90 100 "I 4 60 4.80 5 00 5 20

08068.D 041202SCAN.M Tue Apr 16 13:56:51 2002 Page 8

NYC-WTC_000046824

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NYC-WTC_000046824Source: NYC Law Department, mirrored locally

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