GCMS analysis results for sample AE08066, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting the GCMS analysis of sample AE08066 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046786–000046798

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C : \MSDCHEM\1\DATA\020415\08066.D Vial: 23 Acq On : 16 Apr 2002 4:47 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.120 3 7 11 BV 2 10156 130892 0.30% 0.058% 2 3.150 11 12 16 W 3 2646 32077 0.07% 0.014% 3 3.361 41 48 55 PV 3 6553 92735 0.21% 0.041% 4 3.573 80 84 86 W 4 1917 21640 0.05% 0.010% 5 3.643 92 96 101 PV 9758 136016 0.31% 0.060%

6 3.772 101 118 123 W 3 5204 206621 0.47% 0.091% 7 3.814 123 125 128 W 4 2264 29173 0.07% 0.013% 8 3.849 128 131 143 W 7 1676 31938 0.07% 0.014% 9 4.301 204 208 211 W 3 2204 29234 0.07% 0.013% 10 4.789 288 291 296 PV 4 2367 37907 0.09% 0.017%

11 4.883 301 307 312 W 6 2410 52416 0.12% 0.023% 12 5.059 334 337 343 W 5 2005 33045 0.07% 0.015% 13 5.136 346 350 362 W 7 6722 139223 0.31% 0.062% 14 5.459 403 405 407 W 3 1767 15009 0.03% 0.007% 15 5.964 486 491 4 97 PV 14262 262497 0.59% 0.116%

16 6.029 497 502 515 W 17846 357585 0.81% 0.158% 17 9.719 1126 1130 1132 PV 3 1855 17681 0.04% 0.008% 18 9.989 1167 1176 1195 PV 1652264 28335493 64.09% 12.518% 19 10.312 1227 1231 1235 PV 3 1465 21782 0.05% 0.010% 20 11.910 1486 1503 1509 W 5 2619 56017 0.13% 0.025%

21 12.457 1590 1596 1600 W 2 3096 47442 0.11% 0.021% 22 13.485 1755 1771 1786 PV 2181963 37783065 85.46% 16.692% 23 13.585 1786 1788 1790 W 1501 13401 0.03% 0.006% 24 13.632 1790 1796 1802 W 2 4713 87373 0.20% 0.039% 25 15.759 2150 2158 2162 PV 2 2507 51394 0.12% 0.023%

26 16.799 2326 2335 2343 W 4 3377 72251 0.16% 0.032% 27 18.632 2636 2647 2665 PV 2482261 44213456 100.00% 19.532% 28 20.600 2974 2982 2991 PV 208665 3538123 8.00% 1.563% 29 22.645 3319 3330 3338 PV 3 11851 241194 0.55% 0.107% 30 23.021 3381 3394 3413 PV 2 2307951 43899744 99.29% 19.394%

31 23.174 3413 3420 3430 W 16033 368733 0.83% 0.163% 32 25.160 3749 3758 3764 W 2059 43396 0.10% 0.019% 33 30.882 4720 4732 4764 PV 2 1814314 37831125 85.56% 16.713% 34 31.076 4764 4765 4769 W 3 4020 56532 0.13% 0.025% 35 31.106 4769 4770 4776 W 3 3274 70017 0.16% 0.031%

36 31.458 4822 4830 4844 W 4 6419 227247 0.51% 0.100% 37 31.552 4844 4846 4848 W 2122 20420 0.05% 0.009%

08066.D 041202SCAN.M Tue Apr 16 13:55:42 2002 Page 1

NYC-WTC_000046790

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NYC-WTC_000046790Source: NYC Law Department, mirrored locally

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GCMS results for sample AE08069, Apr 2002 · Box DEP Box 27

NYC-WTC_000046841

Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.

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