GCMS analysis results for sample AE08065, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08065 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046771–000046785

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020415\08065.D Vial: 22 Acq On : 16 Apr 2002 3:59 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.138 3 10 32 BV 3 24007 458780 0.84% 0.162% 2 3.379 35 51 57 PV 10231 158747 0.29% 0.056% 3 3.579 77 85 92 PV 7 2988 50739 0.09% 0.018% 4 3.655 92 98 106 PV 15543 247276 0.46% 0.087% 5 3.749 106 114 117 W 6 3643 66704 0.12% 0.024%

6 3.784 117 120 127 W 2 5280 77760 0.14% 0.027% 7 4.207 186 192 205 PV 7 2271 77757 0.14% 0.027% 8 4.295 205 207 219 PV 5 2665 68793 0.13% 0.024% 9 4.789 283 291 296 W 6 3431 72117 0.13% 0.025% 10 4.883 304 307 314 W 5 4477 88021 0.16% 0.031%

11 4.995 321 326 329 W 5 2077 34519 0.06% 0.012% 12 5.059 333 337 346 PV 7 2466 57225 0.11% 0.020% 13 5.142 346 351 358 W 4 10394 198774 0.37% 0.070% 14 5.964 486 491 498 PV 20674 361836 0.67% 0.128% 15 6.035 498 503 515 W 31397 558133 1.03% 0.197%

16 7.498 748 752 754 PV 3 1783 20912 0.04% 0.007% 17 8.861 965 984 989 W 6 3030 69583 0.13% 0.025% 18 9.636 1112 1116 1122 PV 5 2147 41770 0.08% 0.015% 19 9.719 1125 1130 1138 PV 5 1932 42954 0.08% 0.015% 20 9.989 1162 1176 1188 PV 2013457 33984244 62.59% 11.994%

21 10.312 1224 1231 1241 W 5 1889 38737 0.07% 0.014% 22 10.424 1247 1250 1254 W 3 1845 25394 0.05% 0.009% 23 11.910 1490 1503 1507 W 3 3450 80142 0.15% 0.028% 24 12.081 1526 1532 1536 PV 3 2330 48461 0.09% 0.017% 25 12.457 1589 1596 1610 W 3 4710 101812 0.19% 0.036%

26 12.568 1610 1615 1622 W 4 2497 53418 0.10% 0.019% 27 13.485 1761 1771 1787 PV 2579816 45440424 83.69% 16.038% 28 13.638 1791 1797 1805 W 6933 128163 0.24% 0.045% 29 13.879 1831 1838 1844 W 7 2674 55861 0.10% 0.020% 30 15.753 2153 2157 2163 W 3 2376 40077 0.07% 0.014%

31 15.953 2184 2191 2197 PV 3 1842 32902 0.06% 0.012% 32 16.799 2330 2335 2344 W 3 ■ 3307 61158 0.11% 0.022% 33 18.632 2634 2647 2667 PV 3043396 54295255 100.00% 19.163% 34 19.020 2703 2713 2723 PV 4 1550 43573 0.08% 0.015% 35 20.201 2911 2914 2924 W 2 1732 35192 0.06% 0.012%

36 20.600 2972 2982 2993 PV 249161 4341738 8.00% 1.532% 37 21.458 3124 3128 3137 W 3 2005 29214 0.05% 0.010%

08065.D 041202SCAN.M Tue Apr 16 13:54:41 2002 Page 1

NYC-WTC_000046775

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NYC-WTC_000046775Source: NYC Law Department, mirrored locally

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