GCMS analysis results for sample AE09099, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR2302\9097.D Vial: 22 Acq On : 24 Apr 2002 11:54 am Operator: Sample : gc/ms scan 4/17 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.183 339 342 372 rVB 301563 768336 21.71% 4.257% 2 12.213 775 781 797 rBV 995686 2463702 69.60% 13.649% 3 15.839 1170 1176 1186 rBV 1527110 3129709 88.42% 17.338% 4 21.145 1748 1754 1766 rBV 1765640 3539572 100.00% 19.609% 5 23.284 1980 1987 1992 rBV 196276 379597 10.72% 2.103%

6 25.589 2231 2238 2249 rBV 1614754 3425127 96.77% 18.975% 7 33.640 3108 3115 3131 rBV2 1079744 2437191 68.86% 13.502% 8 33.860 3134 3139 3149 rVB 68816 159344 4.50% 0.883% 9 37.872 3566 3576 3590 rBV2 587302 1748231 49.39% 9.685%

Sum of corrected areas: 18050809

9097.D GCMS0412.M Wed Apr 24 12:45:33 2002

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