GCMS reference results for sample AE09152, April 2002

Z - o § Quantitation Report (QT Reviewed) — Z Oo Data File : C:\MSDCHEM\1\DATA\020424\0417REF1.D Vial: 7 - O o © o o Acq On : 24 Apr 2002 3:46 pm Operator: Nefliu CD Sample : 04/17 ref Inst Instrumen O O Mise : Multiplr: 1.00 C O MS Integration Params: events.e o Quant Time: May 3 10:56 2002 Quant Results File: SCAN020424 . RES “0 o

Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (RTE Integrator) 3 d Title : Method 508 GC/MS Scan o Q Last Update : Wed Apr 24 08:54:34 2002 C 3 Response via : Initial Calibration ■ CD Abundance TIC: 0417REF1.D 5000000

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I Q li 8 5236 g28 1 2 96 NE 2 ! J 1000000 28:815 8 w as r 1 o 1 N Z

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5 500000 I

0-—T ---------------------- UU UU L A Uii UJ 1 —U JL Time—> 4.00 6.00 8.00 10.00 '12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 ■42.00 44.00 46.00

0417REF1.D SCAN020424.M Fri May 03 10:57:26 2002 Page 3