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GCMS calibration results for sample AE09334, April 2002

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Laboratory report showing GCMS calibration data for sample AE09334 generated on April 25-26, 2002.

NYC-WTC_000046351–000046359

Folder label: “GCMS X 5/7/02 A 5/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2 502\9334.D Vial: 11 Acq On : 25 Apr 2002 10:26 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 7:47 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.65 178 107 N.D. 35) Anthracene 25.58 178 499 N.D. 36) Di-n-butylphthalate 27.55 149 3078 N.D. 37) Fluoranthene 0.00 202 0 N.D. 40) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.64 228 3120 N.D. 43) Bis(2-ethylhexyl)phthalate 33.86 149 36222 1.06 ug/1 99 44) Chrysene 33.64 228 3121 N.D. 46) Di-n-Octylphthalate 0.00 149 0 N.D. 47) Benzo(b)fluoranthene 0.00 252 0 N.D. 48) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 9) Benzo(a)pyrene 37.87 252 3427 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 9334.D GCMS0412.M Fri Apr 26 07:47:47 2002 Page 2

NYC-WTC_000046352

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NYC-WTC_000046352Source: NYC Law Department, mirrored locally

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