GCMS sample analysis results for unknowns, May 2002

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Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE09579 on May 17, 2002.

NYC-WTC_000046238–000046248

Folder label: “GCMS X 5/7/02 A 5/9/02”

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0802\9579.D Vial: 16 Acq On 9 May 2002 1:15 am Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 15:45 2002 Quant Results File: GCMS0507 .ES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 448674 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1625405 40.00 ug/1 0.00 17) Acenaphthene-diO 21.13 164 873631 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1168352 40.00 ug/1 0.00 38) Chrysene-dl2 33.63 240 582083 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 327577 40.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 23.27 209 36220 8.33 ug/L 0.00 Spiked Amount 10.000 Recovery = 83.30%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 849 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 723 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.64 178 503 N.D.

(#) = qualifier out of range (m) = manual integration 9579.D GCMS0507.M Thu May 09 15:46:34 2002 Page 1

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GCMS analysis results for sample AE09585, May 2002 · Box DEP Box 25

NYC-WTC_000046284

Laboratory report documenting GCMS analysis of sample AE09585 conducted on May 17, 2002.

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