GCMS analysis results for sample AE10815, May 2002

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Gas chromatography-mass spectrometry report for sample AE10815 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046094–000046111

Folder label: “GCMS X 5/7/02 A 5/15/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\051402\10815.D Vial: 25 Acq On : 15 May 2002 9:55 am Operator: Mclean Sample : 5/7 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 16 14:16:51 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 16 12:34:41 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.94 152 6880723 40.00 ug/L 0.00 10) Napthalene-d8 13.43 136 27369097 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.57 164 14790774 40.00 ug/L 0.00 29) Phenanthranene-dlO 22.95 188 21438990 40.00 ug/L 0.00 37) Chrysene-dl2 30.81 240 15281340 40.00 ug/L 0.00 43) Perylene-dl2 34.71 264 9761242 40.00 ug/L 0.00

System Monitoring Compounds 2 7) TCMX 20.54 209 891664 9.93 ug/L 0.00 Spiked Amount 10.000 Recovery 99.30%

Target Compounds Qvalue 2) n-nitros-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-nitroso-di-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 12.94 93 3097 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Napthalene 13.48 128 36564 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) 2-Chloronaphthalene 0.00 162 0 N.D. 19) Dimethylphthalate 0.00 163 0 N.D. 20) 2,6-Dinitrotoluene 0.00 165 0 N.D. 21) Acenapthylene 0.00 152 0 N.D. 22) Acenapthalene 0.00 153 0 N.D. 23) 2,4-Dinitrotoluene 0.00 165 0 N.D. 24) Diethylphthalate 20.14 149 14318 N.D. 25) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 26) Fluorene 0.00 166 0 N.D. 28) Azobenzene 0.00 77 0 N.D. 30) Nnitrosodiphenylamine 20.54 169 17359 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 25.09 149 38402 N.D.

(#) = qualifier out of range (m) = manual integration 10815.D 050102.M Thu May 16 14:17:06 2002 Page 1

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