GCMS analysis results for sample AE10814, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10814 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046081–000046093

Folder label: “GCMS X 5/7/02 A 5/15/02”

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OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document

• Data File C:\MSDCHEM\1\DATA\051402\10814.D Vial: 24 Acq On 15 May 2002 9:06 am Operator: Mclean Sample 5/7 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.114 3 6 16 BV 5 2453 50536 0.09% 0.018% 2 3.532 73 77 89 PV 8 2474 57882 0.11% 0.021% 3 3.696 96 105 106 W 5 2950 62956 0.12% 0.023% 4 3.731 106 111 113 W 6 2901 58053 0.11% 0.021% 5 3.749 113 114 117 W 2 2856 34396 0.06% 0.012%

6 4.248 195 199 203 W 4 3321 55673 0.10% 0.020% 7 4.337 203 214 218 W 7 3920 107801 0.20% 0.039% 8 4.572 250 254 258 PV 6 1687 19964 0.04% 0.007% 9 5.042 329 334 339 PV 6 1847 31286 0.06% 0.011% 10 5.406 392 396 413 W 3 4920 123516 0.23% 0.044%

11 5.653 433 438 446 W 9 2350 75114 0.14% 0.027% 12 5.841 466 470 480 W 6 2243 41496 0.08% 0.015% 13 5.970 484 492 513 W 592286 10399297 19.54% 3.731% 14 6.099 513 514 516 W 2 1414 10608 0.02% 0.004% 15 7.163 690 695 703 PV 4 2789 57436 0.11% 0.021%

16 7.733 784 792 804 W 3 6058 178936 0.34% 0.064% 17 8.743 958 964 971 W 8 1981 42105 0.08% 0.015% 18 9.254 1043 1051 1056 PV 12246 197626 0.37% 0.071% 19 9.307 1056 1060 1070 W 5 1952 38960 0.07% 0.014% 20 9.936 1153 1167 1187 PV 1961727 36856274 69.23% 13.224%

21 12.404 1577 1587 1607 PV 12730 219058 0.41% 0.079% 22 13.432 1751 1762 1776 PV 2645244 49307210 92.62% 17.691% 23 13.520 1776 1777 1782 W 3 3382 47183 0.09% 0.017% 24 13.585 1782 1788 1794 W 2 9325 173240 0.33% 0.062% 25 13.831 1817 1830 1841 W 6 2205 58753 0.11% 0.021%

26 14.049 1862 1867 1874 PV 5 1705 27841 0.05% 0.010% 27 15.482 2102 2111 2121 W 2 9093 149828 0.28% 0.054% 28 15.700 2135 2148 2157 PV 5 1932 54060 0.10% 0.019% 29 16.746 2321 2326 2335 PV 5 4054 92426 0.17% 0.033% 30 18.232 2573 2579 2585 W 2 10530 160800 0.30% 0.058%

31 18.567 2624 2636 2667 BV 2683385 53233957 100.00% 19.100% 32 20.535 2954 2971 2981 BV 410509 7496810 14.08% 2.690% 33 20.682 2989 2996 3009 W 2 8839 129227 0.24% 0.046% 34 21.758 3173 3179 3189 PV 3 2004 40891 0.08% 0.015% 35 22.580 3310 3319 3330 PV 19988 358613 0.67% 0.129%

36 22.792 3349 3355 3366 W 2 4642 71932 0.14% 0.026% 37 22.956 3370 3383 3402 PV 2 2389457 51020762 95.84% 18.306%

10814.D 050102.M Thu May 16 14:16:30 2002 Page 1

NYC-WTC_000046086

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NYC-WTC_000046086Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE10815, May 2002 · Box DEP Box 25

NYC-WTC_000046094

Gas chromatography-mass spectrometry report for sample AE10815 showing detection of unknown compounds and surrogate recovery.

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