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GCMS analysis results for sample AE10704, May 20 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report for sample AE10704 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045793–000045810

Folder label: “GCMS X 5/3/02 A 5/13/02

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Scanned page image, NYC-WTC_000045810
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NYC 9/11 Public Portal Document

Operator ID: Nefliu Date Acquired: 14 May 2002 2:23 am Data File: C:\MSDCHEM\1\DATA\020513\10704.D Name: sample Mise : Method: C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title: Method 508 GC/MS Scan Library Searched: C:\DATABASE\nist98.1

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone — Acetonitrile, die 3.66 0.6 ug/1 54737 1 11.38 3888190 40.0 • 2-Pentanone, 4-hy 6.16 14.1 ug/1 1371280 1 11.38 3888190 40.0 Hept asi l oxane,—1, 28.36 0.4 ug/1 54873 4 31.72 5356370 40.0 -Anthracene, 2 -met 31.09 0.3 ug/1 46709 4 31.72 5356370 40.0 Anthracene-d10 - 31.96 0.4 ug/1 48682 4 31.72 5356370 40.0 ,1,5,7,7,7Hep 32.20 0.4 ug/1 53976 4 31.72 5356370 40.0 Octasiloxane,—1,2 34.55 0.3 ug/1 40107 4 31.72 5356370 40.0 3-Is oprepoxy= 1.1. 36.28 0.4 ug/1 43002 5 39.94 4355360 40.0 t-Butyldimothyl (2 37.70 0.4 ug/1 42649 5 39.94 4355360 40.0 • Phosphonic acid, 38.54 5.9 ug/1 647211 5 39.94 4355360 40.0 3 -Isopropexy- 11, 38.93 0.4 ug/1 42673 5 39.94 4355360 40.0

10704.D SCAN020507.M Wed May 15 09:01:28 2002 Page 14

NYC-WTC_000045810

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NYC-WTC_000045810Source: NYC Law Department, mirrored locally

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