Gas chromatography-mass spectrometry report for sample AE10703 showing detection of unknown compounds and surrogate recovery.
NYC-WTC_000045778–000045792Folder label: “GCMS X 5/3/02 A 5/13/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020513\10703.D Vial: 14 Acq On : 14 May 2002 1:24 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1
Peak Number 2 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.
6.15 13.29 ug/1 1068360 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual
2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 45 4 Propane, 2-methyl-2-(1-methyleth... Abundance / Scan 523 (6.152 min): 10703.D (-520) (-) 116 C7H160 017348-59-3 33 m/z 43.10 100.00% 4(3
59 5000
101 ■ ■ i ■ 1 1 1 1 1 1 1 1 1 ' 1 1 1 1 1 1 1 1 1 580 6.00 6.20 6.40 ..............................37,1, 53, 69 83 125 m/z 59.10 56.14% ■ ■ i ' ' 1 ■ i 1 1 ■ ■ i 1 ' 1 1 I 1 H ' r I■111i111 1 1 ‘ 1 1 1 i 1 1 ■ 1 i 1 1 1 1 i ' ' 1 1 i 1 1 1 1 i 1 1 n/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109756: 2-Pentanone, 4-hydroxy-4-methyl- 43
5000 59 *II*/IT’*IIIILTTIII11I 5.80 6.00 6.20 6.40 m/z 58.05 17.75% ...... 25,,,^37 , 93 83 — 93 101 I ' । | I I i । | । | I r | i i i I | I 11111 iji 1 I 1 ■ 1 1 i 1 1 ■ 1 i ' 1 1 1 i ‘ ■ 1 i 1 1 1 ' I 1 ' ■ ■ i 1 1 1 1 l ' ' n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5851:2-Pentanone, 4-hydroxy-4-methyl- 43 - , , । 1 i r-|-[ l "Pi । i i TTt 580 6.00 6.20 6.40 5000 m/Z 101.10 17.55% 59 — 101
m/z—> 27 ,< , । 37 V’I ii 1 1 1 1 1 1 ' I 1 111117 'i | । 10 20 30 40 +53+ 50 60 67 77 83 91 IIttI*‘**IUI*I**#1I+I*IIIIIIII1II 70 80 90 100 110 120 130 |
Abundance #109755: 2-Pentanone, 4-hydroxy-4-methyl- 1 43 580 6.00 6.20 6.40 m/ z 41.05 7.87%
5000 59
15 101 1 I 1 25.71,3744 53, I | < • 1 " | ■ ' ■ ■ | 83 i | 1 ' l 1 1 " i 1 ’1 ' 1 | 1 ' 1 I | I 1 ■ l-| i I I I | ! > ■> i | r-r i “maorTrii rrpmrr mlz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40
10703 .D SCAN020507.M Wed May 15 08:59:07 2002 Page 4
NYC-WTC_000045785
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NYC-WTC_000045748
Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046180
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10133 on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043792
Analytical report for sample AE09768 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043806
Analytical report for sample AE09769 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043779
Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024366
Chain of custody record for GCMS analysis of sample AE10236 on May 20, 2002, including surrogate compound data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022526
Laboratory report of GCMS analysis for sample AE11425 conducted on May 29, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024665
Laboratory report documenting GCMS analysis of sample AE11158 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Laboratory report of a GC/MS blank run analyzing volatile organic compounds with results below detection limits in May 2002.
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