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GCMS analysis results, sample AE10701, May 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.

NYC-WTC_000045748–000045760

Folder label: “GCMS X 5/3/02 A 5/13/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020513\10701.D Vial: 12 Acq On : 13 May 2002 11:24 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.123 512 518 520 rBV 27477 39896 0.98% 0.180% 2 6.152 520 523 563 rVB 445810 910353 22.41% 4.099% 3 11.376 1400 1412 1430 rBV 1148797 2946912 72.54% 13.270% 4 16.534 2275 2290 2305 rBV 1356716 3674989 90.47% 16.548% 5 24.455 3621 3638 3660 rBV 1321668 3839201 94.51% 17.288%

6 27.533 4149 4162 4174 rBV3 196220 558083 13.74% 2.513% 7 28.368 4292 4304 4316 rVB3 10423 35272 0.87% 0.159% 8 31.088 4759 4767 4781 rVB4 11667 34088 0.84% 0.153% 9 31.717 4853 4874 4896 rBV2 1360614 4062266 100.00% 18.292% 10 31.958 4905 4915 4925 rVB3 11918 35188 0.87% 0.158%

11 32.193 4939 4955 4965 rBV4 10548 35799 0.88% 0.161% 12 39.937 6262 6273 6290 rBV2 1773123 3552497 87.45% 15.997% 13 43.151 6809 6820 6845 rBV2 1249579 2483320 61.13% 11.182%

Sum of corrected areas: 22207864

10701 .D SCAN020507 .M Wed May 15 08:41:53 2002 Page 1

NYC-WTC_000045752

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NYC-WTC_000045752Source: NYC Law Department, mirrored locally

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