GCMS analysis results for sample AE10610, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10610 including surrogate recovery data in May 2002.

NYC-WTC_000045662–000045681

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\050702\10610.D Vial: 13 Acq On 7 May 2002 10:55 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.555 76 81 88 PV 5 1875 30281 0.06% 0.011% 2 3.714 102 108 112 W 7 1323 32789 0.07% 0.012% 3 3.749 112 114 117 W 5 1131 12261 0.02% 0.004% 4 3.779 117 119 121 PV 3 1146 6615 0.01% 0.002% 5 4.272 197 203 209 PV 5 2869 55739 0.11% 0.020%

6 4.354 209 217 228 W 9381 172105 0.35% 0.063% 7 5.054 331 336 344 PV 6 2300 64066 0.13% 0.023% 8 5.424 395 399 403 W 3 1780 25949 0.05% 0.009% 9 5.976 481 493 519 PV 399082 6947983 14.02% 2.537% 10 7.739 787 793 801 PV 3 3872 83837 0.17% 0.031%

11 9.936 1158 1167 1184 PV 1806371 33705434 68.01% 12.307% 12 10.265 1216 1223 1232 PV 7 2214 48498 0.10% 0.018% 13 11.869 1490 1496 1503 PV 4 2210 41216 0.08% 0.015% 14 12.909 1664 1673 1679 PV 6 1700 51811 0.10% 0.019% 15 13.432 1747 1762 1778 PV 2394621 45482559 91.77% 16.608%

16 13.585 1781 1788 1795 W 2 7602 129338 0.26% 0.047% 17 13.832 1818 1830 1836 BV 6 3572 58082 0.12% 0.021% 18 15.489 2105 2112 2123 W 3 3526 89411 0.18% 0.033% 19 15.700 2143 2148 2155 PV 3 2137 39511 0.08% 0.014% 20 16.746 2316 2326 2334 PV 4 3779 73497 0.15% 0.027%

21 17.386 2430 2435 2445 W 7978 123420 0.25% 0.045% 22 18.232 2571 2579 2588 W 13940 212818 0.43% 0.078% 23 18.573 2625 2637 2653 PV 2471099 49562352 100.00% 18.098% 24 18.967 2692 2704 2707 PV 2 1572 23983 0.05% 0.009% 25 20.324 2928 2935 2943 W 2 6020 109403 0.22% 0.040%

26 20.536 2958 2971 2982 PV 292014 5223424 10.54% 1.907% 27 20.688 2986 2997 3003 W 16398 259870 0.52% 0.095% 28 21.758 3163 3179 3192 W 3 5429 124067 0.25% 0.045% 29 22.580 3309 3319 3338 W 2 20711 396248 0.80% 0.145% 30 22.804 3350 3357 3371 W 9171 158506 0.32% 0.058%

31 22.956 3371 3383 3403 PV 2 2209535 48411388 97.68% 17.677% 32 23.109 3403 3409 3420 W 2 27621 602679 1.22% 0.220% 33 24.684 3670 3677 3683 PV 4705 81457 0.16% 0.030% 34 25.095 3741 3747 3756 PV 3 1632 37335 0.08% 0.014% 35 26.400 3964 3969 3975 W 3 3477 58214 0.12% 0.021%

36 27.140 4083 4095 4102 W 5 6286 121631 0.25% 0.044% 37 27.674 4176 4186 4194 PV 5 3010 67680 0.14% 0.025%

10610.D 050102.M Thu May 09 09:15:05 2002 Page 1

NYC-WTC_000045667

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NYC-WTC_000045667Source: NYC Law Department, mirrored locally

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