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GCMS analysis results for sample AE10609, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.

NYC-WTC_000045643–000045661

Folder label: “GCMS X 5/3/02 A 5/7/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\050702\10609.D Vial: 12 Acq On 7 May 2002 10:06 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 09 09:12:47 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 08 09:53:56 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 25.09 149 25454 N.D. 36) Fluoroanthene 0.00 202 0 N.D. 38) Pyrene 0.00 202 0 N.D. 39) Butylbenzylphthalate 0.00 149 0 N.D. 40) Benzo(a)anthracene 30.81 228 31492 N.D. 41) Bis(2-ethylhexyl)phthalate 31.38 149 15672 N.D. 42) Chrysene 0.00 228 0 N.D. 44) Di-n-octylphthalate 0.00 149 0 N.D. 45) Benzo(b)fluoranthene 0.00 252 0 N.D. 46) Benzo(k)fluoranthene 0.00 252 0 N.D. 47) Benzo(a)pyrene 0.00 252 0 N.D. 48) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 49) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10609.D 050102.M Thu May 09 09:13:33 2002 Page 2

NYC-WTC_000045646

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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