GCMS sample analysis results for AE10606, May 10 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\050702\10606.D Vial: 11 Acq On 7 May 2002 9:17 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.302 32 38 44 PV 3 6561 120752 0.25% 0.046% 2 3.520 71 75 79 PV 5 1872 32140 0.07% 0.012% 3 3.590 83 87 95 W 2 13789 243297 0.50% 0.093% 4 3.720 95 109 116 W 3 8012 297101 0.61% 0.114% 5 3.772 116 118 129 W 9 3276 119005 0.24% 0.045%

6 4.243 196 198 205 W 6 3135 54923 0.11% 0.021% 7 4.319 205 211 217 W 10713 201115 0.41% 0.077% 8 5.024 322 331 336 PV 9 4332 104929 0.22% 0.040% 9 5.089 336 342 362 W 9 4619 166355 0.34% 0.064% 10 5.576 413 425 433 PV 7 1785 66182 0.14% 0.025%

11 5.641 433 436 440 W 2 2751 37964 0.08% 0.015% 12 5.970 483 492 52 0 PV 363857 7072566 14.52% 2.704% 13 7.445 738 743 756 W 7 1989 43250 0.09% 0.017% 14 7.738 783 793 799 W 4 4773 108918 0.22% 0.042% 15 8.820 971 977 986 W 4 2571 63833 0.13% 0.024%

16 9.936 1157 1167 1198 PV 1696323 33491368 68.74% 12.804% 17 11.863 1490 1495 1501 W 3 4581 70148 0.14% 0.027% 18 12.039 1518 1525 1535 W 3 2187 43437 0.09% 0.017% 19 13.432 1752 1762 1776 PV 2384694 44779458 91.91% 17.120% 20 13.585 1776 1788 1794 W 7481 161307 0.33% 0.062%

21 13.831 1817 1830 1834 PV 5 4216 71843 0.15% 0.027% 22 15.483 2105 2111 2116 PV 2 4292 67581 0.14% 0.026% 23 15.700 2131 2148 2152 W 3 2569 48064 0.10% 0.018% 24 16.746 2321 2326 2340 W 4 4632 97572 0.20% 0.037% 25 18.232 2571 2579 2587 W 2 16615 266775 0.55% 0.102%

26 18.573 2626 2637 2652 PV 2441096 48722779 100.00% 18.627% 27 18.961 2697 2703 2709 W 5 2067 33867 0.07% 0.013% 28 20.324 2931 2935 2941 PV 3 5470 84738 0.17% 0.032% 29 20.535 2959 2971 2984 W 2 316968 5665385 11.63% 2.166% 30 20.688 2990 2997 3003 W 18748 302813 0.62% 0.116%

31 21.393 3114 3117 3126 W 6 1836 29340 0.06% 0.011% 32 21.758 3169 3179 3195 W 2 11632 265349 0.54% 0.101% 33 22.580 3312 3319 3328 W 2 20353 383782 0.79% 0.147% 34 22.803 3350 3357 3363 W 11657 203703 0.42% 0.078% 35 22.956 3370 3383 3403 PV 2 2177244 46957427 96.38% 17.953%

36 23.109 3403 3409 3420 W 2 28237 628883 1.29% 0.240% 37 24.684 3672 3677 3687 W 4 5761 119166 0.24% 0.046%

10606.D 050102.M Thu May 09 09:11:41 2002 Page 1

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