GCMS analysis results for sample AE09449, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\MAYO 8 02\9449.D Vial: 10 Acq On 8 May 2002 7:22 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 13.35 ug/1 878329 1,4-Dichlorobenzene-d4 12.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pent a: ne, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 N,N' -Bi/ (2-methyl-2-nitrosopentan-4 258 C12H22N2O4 094514-30-4 9 3 CH2=C CH2C(0)OCH3 100 C5H802 003724-55-8 9 4 Aceto e 58 C3H60 000067-64-1 7 Abundance - Scan 340 (8.160 min): 9449. D (-) m/z 43.05 100.00% 43

5000 59 । । । । i । । । 1tll । iiii । । । i । । । 101 7.80 8.00 8.20 8.40 8.60 0 ■ 1 i ■ ■ ■ ■ । 1

m/z->_____ 10 20 — 374 ——53, 67______ 83 1 1 I ' ' ' 1 I 30 40 50 60 70 80 90 100 110 120 130 i—| i— । । । | F 1T—”u—v I — I i i ■ । i i m/z 59.10 42.74% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 16.50% 27 ■' । 1 ■ ■ ■ ।' m/z->______10 20 - 30 40 +49 50 60 70 80 — 83 90 101 | 100 110 120 130 Abundance #35454: N,N'-Bis(2-methyl-2-nitrosopentan-4-one) 43 II I I I I 1 I I I I I I I I I 1 I I I I I ] I 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.90%

99 15 27 56 72r ITI83 T — i I l pi i l r ~31"7 “I 1" <“l | I “l“ I I I I I I I I । । । । । । । । । । 130 । i | । r

m/z-> 10 20 30 40 50 60 80 70 90 100 110 120 130 Abundance #1448: CH2=CHCH2C(O)OCH3 I I I I I I I I I I I I I I I I I ] I I > I I I

43 7.80 8.00 8.20 8.40 8.60 m/z 41.15 7.05%

5000 A 58 ............................. 37 , I 72 100 ■ 1 i 1 1 ' 1 i 1 1 ■ 1 i 1 1 1 1 i1 ’ 1 1 [ ' 1 '1 i ■ 1 1 1 ? ( ' 1 r ' 1 1 i 1 ■ ■ 1 I - 1 1 1 | 1 1 1 1 | '' 1 1 | T T M-TT । । I P —PPTP—i—।—r* m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40 8.60

9449.D GCMS0507.M Thu May 09 14:43:17 2002 Page 1

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