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GCMS analysis results for sample AE10608, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE10608 including surrogate recovery data conducted on May 15, 2002.

NYC-WTC_000045434–000045442

Folder label: “GCMS X 5/3/02 A 5/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAY0802\10608.D Vial: 7 Acq On 8 May 2002 4:26 pm Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.157 336 340 346 rBV 482291 950349 26.13% 5.560% 2 12.189 775 780 796 rBV 1175313 2620988 72.05% 15.334% 3 15.827 1170 1177 1194 rBV 1612994 3278196 90.12% 19.179% 4 21.133 1749 1756 1771 rBV 1746352 3637679 100.00% 21.282% 5 23.268 1981 1989 1998 rBV2 178619 391848 10.77% 2.292%

6 25.577 2234 2241 2251 rW2 1505294 3206453 88.15% 18.759% 7 33.632 3113 3120 3134 rBV 796336 1783711 49.03% 10.435% 8 37.856 3573 3581 3601 rBV2 419693 1223646 33.64% 7.159%

Sum of corrected areas: 17092870

10608 .D GCMS0507.M Thu May 09 14:42:25 2002

NYC-WTC_000045439

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NYC-WTC_000045439Source: NYC Law Department, mirrored locally

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