GCMS analysis results for sample AE10437, May 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAY1002\10437.D Vial: 34 Acq On : 11 May 2002 10:16 pm Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 13.23 ug/1 788927 1,4-Dichlorobenzene-d'4 12.16

Hit# of Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4 - hydroxy-4-methyl - 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3/5-Hexen-2 -one 98 C6H10O 000109-49-9 7 A Acetone________ 58 C3H60 000067-64-1 7 bundance Scan 338 (8.138 min): 10437.D (-) m/z 43.05 1.00.00% 43

5000 59

101 1‘111+++1111111+1‘‘‘I‘ 7.80 8.00 8.20 8.40 । ' । 38 i ' । ' ' ' ri 1n1t-du ++ 53 , 69 83 , I m/z 59.10 43.52% m/z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 " । । ' । ■ i ■ >' ' । 1nn । j । , 59 7.80 8.00 8.20 8.40 m/z 58.10 16.42% 27 101 83 I I PT +49 I 1 1 1 ' i 1,1 1 1 111 ' 1 1 I J' ' ' ' | ' mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 1 1 । 1 1 1 1 । 1 1 1 1 । . . ■ । । 1 1 1 1 । 1 7.80 8.00 8.20 8.40 5000 m/z 101.15 14.06%

58 72 100 38,4 IIIIIIIIII* m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one ■ > । ■ i - ■ ■ ■ j . . . . । . . . . । . 43 7.80 8.00 8.20 8.40 m/z 41.00 6.58%

5000

55 15 27 50 | 83 98 ... I ... 1....38, ■ ■ । । । ■ i • ■ . . j . . . . -TT । । . । i । । । . . । । 1111**111+14 n/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

10437.D GCMS0510.M Thu May 16 12:03:47 2002 Page 1

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