GCMS analysis results for sample AE10306, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10306.D Vial: 9 Acq On 8 May 2002 8:19 pm Operator: Mclean Sample 5/1 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L Peak Number 6 2-Hexanone, 5-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.24 ug/L 236756 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone, 5-methyl- 114 C7H140 000110-12-3 /25 2 Acetone 58 C3H60 000067-64-1 16 3 Acetone 58 C3H60 000067-64/1 9 4 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 Abundance Scan 792 (7.733 min): 10306.D (-788) (-) m/ z 43.10 100.00% 43

5000 58 87 36 ii 98 7.40 7.60 7.80 8.00

mfe-> ol 1 ' । 1' 1 • । ■ 1 1 ' ।■1 f +49— 1 1 i 1 ' mm ...................... 10 20 | 1,1 30 40 50 70 80 IlLu 90 60 100 110 120 m/z 58.10 34.85% Abundance #109705: 2-Hexanone, 5-methyl- 4(3

WwMAlw Wyhwhuks 5000 ‘ 1 i ' ' 1 1 i 1 • ■ 1 i 1 ■ ' 1 i 1 1 ‘ ‘ i 58 7.40 7.60 7.80 8.00 27 m/z 87.10 22.30% 1 ' I 1 P | ! I I I I I 71 । .........Ill , , 1 ‘ I1 1 1 1 i ' 85 1 i ' ' ■ 99 114 0! ''i 1 1 1 ■ i ' 1 ■ ■ i 1 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #109708: Acetone N 43 .... |..... |k........ 1 ' i ' 1 ' ■ i 1 1 1 ‘i’ 7.40 7.60 7.80 8.00 5000 m/z 83.00 19.04% 58

27 37 I 52 0+ ................ .. ''bi' i ''I'J 1 ' ' I " m/z-> Abundance 10 20 30 40

43 50 60 #5734: Acetone 70 80 90 100 110 120 ........ Ill......... 7.40 7.60 7.80 8.00 m/z 59.10 16.58%

5000 15 58 A fi

27 0 ' " I ' I1" I ' litpe ' rrl i I I [ I l t 111/1/1171/111*/1/*1*’’’1’1*I’’’I’ ■ ' i ■ ' 1 1 i ' ' 1 1 I ' 1 ' 1 i 1 ' ■ 1 i m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 7.40 7.60 7.80 8.00

10306.D 050102.M Thu May 09 13:51:41 2002 Page 9

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