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GCMS analysis results for unknown compounds, sample AE09093, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\050802\9093 .D Vial: 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.132 4 9 19 BV 4 5293 100727 0.18% 0.033% 2 3.549 77 80 88 PV 8 3865 73956 0.13% 0.024% 3 3.702 95 106 109 PV 5 3171 91388 0.16% 0.030% 4 3.737 109 112 117 W 6 3941 92899 0.16% 0.030% 5 3.778 117 119 123 W 5 3193 53707 0.09% 0.017%

6 3.914 139 142 149 W 8 2998 79207 0.14% 0.026% 7 4.172 183 186 190 W 5 2876 48469 0.08% 0.016% 8 4.278 198 204 212 W 7 3656 88052 0.15% 0.028% 9 4.354 212 217 222 W 7 2462 51379 0.09% 0.017% 10 4.583 253 256 261 PV 6 2196 30475 0.05% 0.010%

11 4.954 313 319 328 PV 20750 368965 0.64% 0.119% 12 5.030 328 332 344 W 2 7014 202542 0.35% 0.065% 13 5.382 381 392 395 W 6 3342 104437 0.18% 0.034% 14 5.424 395 399 407 W 4 6587 146580 0.26% 0.047% 15 5.594 417 428 430 W 7 2392 70901 0.12% 0.023%

16 5.641 430 436 445 W 5 11401 251377 0.44% 0.081% 17 5.847 466 471 478 W 4 2569 42367 0.07% 0.014% 18 5.976 485 493 522 W 651131 11315941 19.77% 3.656% 19 6.951 654 659 666 W 5 1680 41849 0.07% 0.014% 20 7.739 789 793 805 PV 2 7845 230591 0.40% 0.074%

21 8.109 849 856 864 PV 6 2513 49562 0.09% 0.016% 22 8.749 958 965 972 BV 4 3343 64156 0.11% 0.021% 23 9.254 1046 1051 1054 PV 4 1801 28378 0.05% 0.009% 24 9.307 1058 1060 1064 W 4 2158 33038 0.06% 0.011% 25 9.936 1149 1167 1188 PV 2123873 39621532 69.24% 12.800%

26 12.404 1583 1587 1597 W 3 2310 34975 0.06% 0.011% 27 13.432 1748 1762 1782 PV 2821393 53081551 92.76% 17.148% 28 13.585 1782 1788 1793 W 2 9157 161476 0.28% 0.052% 29 15.700 2140 2148 2155 BV 2 2378 36498 0.06% 0.012% 30 16.746 2321 2326 2334 PV 2 4786 80328 0.14% 0.026%

31 18.567 2625 2636 2658 PV 2928376 57226415 100.00% 18.487% 32 18.961 2697 2703 2715 W 5 2773 61994 0.11% 0.020% 33 20.536 2959 2971 2984 W 397068 7265477 12.70% 2.347% 34 21.393 3106 3117 3127 W 6 2665 54660 0.10% 0.018% 35 22.580 3312 3319 3329 W 3 22033 414925 0.73% 0.134%

36 22.956 3371 3383 3403 PV 2 2664734 55361400 96.74% 17.885% 37 23.109 3403 3409 3431 W 2 28379 761436 1.33% 0.246%

9093.D 050102.M Thu May 09 13:33:16 2002 Page 1

NYC-WTC_000044907

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NYC-WTC_000044907Source: NYC Law Department, mirrored locally

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