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GCMS analysis results for sample AE10061, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE10061 conducted on May 14, 2002, including surrogate recovery data.

NYC-WTC_000044203–000044214

Folder label: “GCMS X 4/26/02 A 5/8/02

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Scanned page image, NYC-WTC_000044205
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NYC 9/11 Public Portal Document

' Data File C:\MSDCHEM\l\DATA\020507\10061.D Vial: 25 Acq On 8 May 2002 11:46 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:53:54 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 440281 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1666517 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 897864 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1529756 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1245366 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 801267 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.53 207 56360 7.86 ug/1 -0.04 Spiked Amount 10.000 Recovery = 78.60% Target Compounds Qvalue 35) Di-n-butylphthalate 34.80 149 4925 0.10 ug/1 84 43) Bis(2-ethylhexyl)phthalate 40.52 149 91988 3.45 ug/1 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10061.D SCAN020507 .M Thu May 09 09:55:05 2002 Page 1

NYC-WTC_000044205

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NYC-WTC_000044205Source: NYC Law Department, mirrored locally

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