GCMS analysis results, sample AE09967, May 2002

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38 13.432 1752 1762 1783 PV 2204454 41159142 91.05% 16.622% 39 13.585 1783 1788 1800 W 3 6689 135493 0.30% 0.055% . 40 14.055 1860 1868 1873 W 4 1909 34864 0.08% 0.014%

41 14.613 1957 1963 1966 PV 1653 18233 0.04% 0.007% 42 15.700 2140 2148 2152 PV 2 2430 52780 0.12% 0.021% 43 16.746 2320 2326 2333 W 4 4156 87035 0.19% 0.035% 44 18.379 2600 2604 2608 W 2 1431 17877 0.04% 0.007% 45 18.573 2626 2637 2651 PV 2320541 45205510 100.00% 18.256%

46 18.661 2651 2652 2658 W 4 2253 45233 0.10% 0.018% 47 18.820 2673 2679 2684 W 4 2228 47207 0.10% 0.019% 48 18.967 2696 2704 2709 W 4 2351 55606 0.12% 0.022% 49 20.142 2900 2904 2913 W 3 4056 91581 0.20% 0.037% 50 20.324 2931 2935 2941 W 3 3762 71793 0.16% 0.029%

51 20.541 2957 2972 2980 W 309581 5675521 12.55% 2.292% 52 21.205 3082 3085 3091 PV 3 1837 35127 0.08% 0.014% 53 21.393 3114 3117 3126 W 4 2419 55936 0.12% 0.023% 54 21.758 3171 3179 3186 W 6 4946 121181 0.27% 0.049% 55 22.580 3312 3319 3334 W 3 18277 380344 0.84% 0.154%

56 22.956 3371 3383 3403 BV 2 2112615 44314418 98.03% 17.896% 57 23.109 3403 3409 3427 W 25644 707191 1.56% 0.286% 58 23.732 3508 3515 3522 W 2 4102 99146 0.22% 0.040% 59 23.873 3535 3539 3541 PV 2 1711 21505 0.05% 0.009% 60 24.102 3572 3578 3580 W 2 1683 32818 0.07% 0.013%

61 25.095 3741 3747 3756 W 3 8768 201064 0.44% 0.081% 62 25.906 3881 3885 3888 W 1673 24615 0.05% 0.010% 63 26.540 3988 3993 3997 W 3 2800 49819 0.11% 0.020% 64 27.175 4095 4101 4111 PV 4 3018 75761 0.17% 0.031% 65 29.884 4559 4562 4568 PV 1942 32747 0.07% 0.013%

66 29.983 4568 4579 4584 W 4 1744 56196 0.12% 0.023% 67 30.066 4584 4593 4599 W 4 2357 65227 0.14% 0.026% 68 30.360 4639 4643 4646 PV 1563 19174 0.04% 0.008% 69 30.812 4708 4720 4750 W 2 1609720 38452860 85.06% 15.529% 70 31.000 4750 4752 4759 W 5 7112 164249 0.36% 0.066%

71 31.053 4759 4761 4764 W 2 4713 71036 0.16% 0.029% 72 31.382 4810 4817 4825 W 5 7438 212183 0.47% 0.086% 73 31.776 4882 4884 4888 W 1961 16506 0.04% 0.007% 74 33.938 5251 5252 5256 W 1493 14170 0.03% 0.006% 75 34.707 5372 5383 5431 PV 2 1064261 27784120 61.46% 11.221%

76 34.995 5431 5432 5435 W 3 5164 54973 0.12% 0.022% 77 35.019 5435 5436 5438 W 2 3814 40449 0.09% 0.016% 78 35.036 5438 5439 5448 W 6 3947 104078 0.23% 0.042% 79 35.354 5491 5493 5498 PV 2 1388 12940 0.03% 0.005% 80 36.041 5606 5610 5613 PV 2 1765 18723 0.04% 0.008%

81 36.076 5613 5616 5622 W 4 2116 33776 0.07% 0.014% 82 36.182 5630 5634 5636 W 1965 25026 0.06% 0.010% 83 36.470 5680 5683 5686 W 2497 27519 0.06% 0.011% 84 37.422 5841 5845 5848 PV 2229 22752 0.05% 0.009% 85 37.457 5848 5851 5854 W 2 2102 28419 0.06% 0.011%

86 38.568 6038 6040 6043 W 2 2012 19729 0.04% 0.008% 87 39.584 6211 6213 6222 W 3 1491 29401 0.07% 0.012%

9967.D 050102.M Tue May 07 15:45:27 2002 Page 2

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