GCMS analysis results, sample AE09771, May 2002

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Laboratory report for sample AE09771 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000043893–000043918

Folder label: “GCMS X 4/25/02 A 5/7/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\050602\9771.D Vial: 24 Acq On 7 May 2002 6:25 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.526 73 76 83 PV 5 2523 43239 0.13% 0.023% 2 3.720 95 109 112 W 6 9726 327082 0.95% 0.171% 3 3.761 112 116 121 W 6 9203 280068 0.81% 0.147% 4 3.802 121 123 125 W 3 8927 124624 0.36% 0.065% 5 3.837 125 129 136 W 6 8894 326849 0.95% 0.171%

6 3.920 136 143 145 W 5 8614 242507 0.70% 0.127% 7 4.008 152 158 161 W 5 8619 241299 0.70% 0.126% 8 4.249 196 199 202 W 3 8613 155370 0.45% 0.081% 9 4.331 209 213 216 W 5 7895 172460 0.50% 0.090% 10 4.554 249 251 261 W 6 6483 232170 0.67% 0.122%

11 5.036 327 333 341 W 7 6404 229110 0.66% 0.120% 12 5.230 364 366 368 W 2 4038 53678 0.16% 0.028% 13 5.829 465 468 473 W 5 3583 75452 0.22% 0.040% 14 5.964 483 491 519 W 400338 7355585 21.34% 3.855% 15 7.733 787 792 801 VV 6 5138 142599 0.41% 0.075%

16 8.115 853 857 860 W 2 2643 34299 0.10% 0.018% 17 8.743 958 964 969 PV 5 2027 41812 0.12% 0.022% 18 8.973 1001 1003 1006 PV 3 1847 16833 0.05% 0.009% 19 9.689 1121 1125 1127 W 4 1696 23351 0.07% 0.012% 20 9.936 1158 1167 1188 W 1267154 23815514 69.08% 12.481%

21 10.394 1243 1245 1251 PV 4 2012 22803 0.07% 0.012% 22 13.432 1748 1762 1773 PV 1722081 31830967 92.34% 16.682% 23 13.508 1773 1775 1778 W 4 2239 29009 0.08% 0.015% 24 13.579 1783 1787 1800 W 3 5068 113970 0.33% 0.060% 25 14.049 1864 1867 1878 PV 6 1806 46066 0.13% 0.024%

26 14.202 1888 1893 1900 PV 4 1675 29772 0.09% 0.016% 27 15.694 2142 2147 2153 W 5 1689 28476 0.08% 0.015% 28 16.740 2319 2325 2336 PV 4 3748 60677 0.18% 0.032% 29 17.392 2426 2436 2440 PV 1644 42886 0.12% 0.022% 30 18.567 2625 2636 2651 W 1824907 34473305 100.00% 18.067%

31 18.673 2651 2654 2663 W 3 2288 69204 0.20% 0.036% 32 18.967 2693 2704 2710 W 3 2057 56966 0.17% 0.030% 33 20.536 2959 2971 2979 W 260991 4588965 13.31% 2.405% 34 20.618 2983 2985 2987 W 1988 17428 0.05% 0.009% 35 21.405 3110 3119 3123 W 5 1581 37811 0.11% 0.020%

36 22.580 3313 3319 3329 W 4 12090 249384 0.72% 0.131% 37 22.951 3372 3382 3403 PV 2 1589825 33331591 96.69% 17.468%

9771.D 050102.M Tue May 07 15:44:09 2002 Page 1

NYC-WTC_000043898

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NYC-WTC_000043898Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AE09973, May 2002 · Box DEP Box 25

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Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

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