GCMS calibration results, sample AE09771, May 2002

z 2 K Quantitation Report (QT Reviewed) - o % o 2 Data File C:\MSDCHEM\l\DATA\050602\CAL4.D Vial: 10 co — o Acq On 6 May 2002 7:04 pm Operator: Mclean 1 "0 o Sample 50.0 Inst : Instrumen C o O o Mise o Multiplr: 1.00 o' c MS Integration Params: EVENTS.E "0 00 o 00 Quant Time: May 8 13:59 2002 Quant Results File: 050102.RES — 0 O Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) o Q C Title 508 Modified GC/MS scan 3 Last Update Wed May 08 09:53:56 2002 CD

Response via Initial Calibration Abundance TIC: CAL4.D

3500000

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§ ® ■ ■

3000000 2® i ■ g 2 @ J 4' 5& g S ®

2500000 ® ( 8 Z 2 o c o & a s 95 ® ® i Qa 1 i 2 82 g% 2 g 528 d o i 2 c z C 18 ge S C a CC N §s 6 o ] 9u 9o 2 3 ra 2 t 1 o

If J

li g g *■l g o S

2000000 #3 1 84218 8 8 &. 9 •Q O z 1 < C ® & x a a g Q R I§ I g 2

i g g “ Q‘+ 5 T । s C i i ROll wo § 0"2 1 I 8 a I I § 8/80 y a 2 z I co CD CM 1500000 gi i1 I

Is z8 | 5 ! 2x CM CM 3 cm" l ! 8 If % 6 1000000 f gg f I ic X s t

500000 2 1

0 __ __ A T-i 11 1 ~ ] 1 1 1 1 | 1 ‘ 1 1 UUU | 1 1 1 1 | .1 I I t 1 | 1 1 1 । ] । । । I | I t । | IL I I ) । | I ! I । । i i I । ! | 1 । I | r-1 । i । i i ! i । Ji i—i i—[—।—।— —i— —t—।—(—i —r~ । । ।

Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

CAL4.D 050102.M Wed May 08 14:00:10 2002 Page 3