Method 508 document fragment, April 2002

NYC 9/11 Public Portal Document

DFTPP J Data File C : \MSDchem\1\DATA\020507\Snapshot\DFTPP . D| Vial: 1 Acq On 7 May 2002 11:26 am 'Operator: Nefliu Sample Inst Instrume Mise Multiplr: 1.00 MS Integration Params: Iscint.e Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan

Abundance TIC: DFTPP.D 5000000

4000000

3000000

2000000

1000000

0 । | 1 J — 1 I ' Time-> 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 Abubase Average of 17.813 to 17.836 min.: DFTPP.D 198 442 300000

77 255 51 127 200000

110 100000 275 224 93

m/z—> 0-37— +4 l+H 40 60 i 148 16718 —+ 241 T r“ 1 । | l r i "r |Tr i 44 226 323 , 346 365 383 403 423 ■r f । । ■ ■ । । ।1 ' 1 i 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 । 1 1 1 ' i 1" I'1 1 i 1 ' +rr

Spectrum Information: Average of 17.813 to 17.836 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 54.5 208624 PASS 68 69 0.00 2 0.8 1425 PASS 69 198 0.00 100 49.4 189221 PASS 70 69 0.00 2 0.5 1016 PASS 127 198 40 60 52.3 200162 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 382656 PASS 199 198 5 9 6.7 25746 PASS 275 198 10 30 25.0 95653 PASS 365 198 1 99 3.2 12406 PASS 441 443 1 100 79.3 49528 PASS 442 198 40 110 85.8 328341 PASS 443 442 17 23 19.0 62485 PASS

DFTPP.D SCAN020507 .M Tue May 07 11:50:36 2002

NYC-WTC_000043748