NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\MAY0 3 02\8837.D Vial: 6
Acq On 3 May 2002 6:56 pm Operator :
Sample RE-EXT. Inst : 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: May 6 9:41 2002 Quant Results File: GCMS0501.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Wed May 01 10:40:31 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0501
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.19 152 485420 40.00 ug/1 -0.02
10) Naphthalene-d8 15.83 136 1772304 40.00 ug/1 -0.02
17) Acenaphthene-diO 21.13 164 959800 40.00 ug/1 -0.02
30) Phenanthrene-diO 25.58 188 1317027 40.00 ug/1 -0.02
38) Chrysene-dl2 33.64 240 765258 40.00 ug/1 -0.02
44) Perylene-dl2 37.87 264 477102 40.00 ug/1 -0.02
System Monitoring Compounds
2 8) TCMX 23.28 209 34187 7.32 ug/L -0.01
Spiked Amount 10.000 Recovery = 73.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.46 74 275 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 13.41 77 206 N.D.
12) Isophorone 14.03 82 744 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.87 128 318 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.61 149 803 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 0.00 168 0 N.D.
32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
33) Hexachlorobenzene 0.00 284 0 N.D.
34) Phenanthrene 25.58 178 376 N.D.
(#) = qualifier out of range (m) = manual integration
8837.D GCMS0501.M Mon May 06 09:42:11 2002 Page 1
NYC-WTC_000043688
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