GCMS analysis results for sample AE09098, May 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0602\9098.D Vial: 6 Acq On 6 May 2002 9:13 pm Operator: Sample Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.16 12.07 ug/1 937682 1,4-Dichlorobenzene-d4 12.20 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 N,N'-Bis(/-methyl-2-nitrosopentan-4 258 C12H22N2O4 094514-30-4 9 3 CH2=CHCH/C(O)OCH3 100 C5H802 003724-55-8 9 4 5-Hexen2-one 98 C6H10O 000109-49-9 7 Abundance F Scan 340 (8.155 min): 9098. D (-) m/ z 43.00 100.00% 43

5000 59

101 7.80 8.00 8.20 8.40 8.60

m/z-> 10 20 30 37—40 53, TTPTT 69 50 60 83 70 80 90 100 ( 110 120 130 m/ z 59.10 42.07% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ' 1 i ’ ' 1 I I I I I > [ 1 ddi I I II' I

59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 16.28% 27 I . 101 TH+ +494 I I I 83 । । mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #35454: N,N’-Bis(2-methyl-2-nitrosopentan-4-one) 43 ......................................... I I I I I < I I I I ■ I I < I I I I I I I I I I

7 80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.04%

99 15 27 56 72 I I I > I I I I I I I I I I I I r I I 'III l-'l ~ l ’ I ’ I I I I > I I I I । । 83 । । i । । । i i 1 i । । । n । । । । i i । 130 i i । । । i r

miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1448: CH2=CHCH2C(O)OCH3 43 780 8.00 8.20 8.40 8.60 m/z 41.05 7.18% 5000

' I 1 1 1 ■ i ■ 56 72 —9— -— m-Pm —3744 1109—99109"3 100 —mmm-— — । । T - i । r -T - "Illi—।—r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40 8.60

9098 .D GCMS0501.M Wed May 08 11:52:08 2002 Page 1

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