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GCMS analysis report for sample AE07002, April 2002

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GCMS results for sample AE07002 showing surrogate recovery and unknown compounds dated April 29, 2002.

NYC-WTC_000043369–000043377

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2402\7002.D Vial: 7 Acq On : 24 Apr 2002 9:39 pm Operator: Sample : gc/ms scan 4/23 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 25 11:01 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.65 178 304 N.D. 35) Anthracene 25.65 178 304 N.D. 36) Di-n-butylphthalate 27.55 149 4948 N.D. 37) Fluoranthene 29.29 202 216 N.D. 4 0) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.64 228 2762 N.D. 43) Bis(2-ethylhexyl)phthalate 33.86 149 1676 N.D. 44) Chrysene 33.70 228 1555 N.D. 46) Di-n-Octylphthalate 35.59 149 396 N.D. 47) Benzo(b)fluoranthene 36.76 252 1800 N.D. 48) Benzo(k)fluoranthene 36.76 252 1800 N.D. 4 9) Benzo(a)pyrene 37.87 252 2494 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 7002.D GCMS0412.M Thu Apr 25 11:02:01 2002 Page 2

NYC-WTC_000043372

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NYC-WTC_000043372Source: NYC Law Department, mirrored locally

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