GCMS surrogate recovery data for sample AE07635, April 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020410\07635.D Vial: 14 Acq On : 10 Apr 2002 10:34 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902. M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library- : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Ethyl Chloride Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.28 0.22 ug/1 151694 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 4 2 2-Butyne-l,4-diol 86 C4H602 000110-65-6 3 3 Krypton 84 Kr 007439-90-9 2 4 Thiophene 84 C4H4S 000110-02-1 2 Abundance Scan 34 (3.279 min): 07635.D (-19) (-) m/z .49.00 100.00% 49 84

5000

40 1'11 ■1'' i'1 " i ‘' 11111'11 1111111 1 3.20 3.30 3.40 3.50 3.60 3.70 0 " |'1 " r' " i ■'" i " '11" " TII] IT rmT' ।.... ।। ।.... ।. " i'1 " r m/z 84.00 79.99% miz-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

28 #107943: Ethyl Chloride MMku 64 5000 3.20 3.30 3.40 3.50 3.60 3.70 49 m/z 86.00 40.09%

UWt 25 35 1215 0 1'I" " I"1111" TTTTT+ 31 |,38____ , ,____ 60 TH....... H 7 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108388: 2-Butyne-1,4-diol 29 39 517 ।11'11 1 1' '11 1 1 111 1' '1 11' 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 51.00 22.56% /" 68 26 51 43

m/z—> —3334 Of ‘' I " " I " " I!'" I 17 FA 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 17477.1.44 Abundance #33829: Krypton 84 3.20 3.30 3.40 3.50 3.60 3.70 m/z 47.00 19.62%

5000 AMWNut, 42 80 0 ............... ... I' ‘' I.........................I I > < ‘ I > > I I I I 1—] '’l' 1 " 11 111'11 111'1111■111111' I 1111111 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.30 3.40 3.50 3.60 3.70

07635.D SCANAPR0902 ,M Thu -Apr 11 14:48:14 2002 Page 3

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