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GCMS surrogate recovery data for sample AE04945, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07634 analyzed on April 30, 2002.

NYC-WTC_000040212–000040229

Folder label: “GCMS X 4/3/02 A 4/10/02

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Scanned page image, NYC-WTC_000040214
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) A

* Data File : C:\MSDCHEM\l\DATA\020410\04945.D Vial: 11 Acq On : 10 Apr 2002 7:47 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 11 15:54:08 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\l-..\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Thu Apr 11 15:44:30 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 10.66 152 2366060 20.00 ug/1 -0.01 10) Naphthalene-d8 15.77 136 8929402 20.00 ug/1 -0.02 17) Acenaphthene-diO 23.66 164 4885691 20.00 ug/1 -0.01 31) Phenanthrene-dlO 30.89 188 7805862 20.00 ug/1 -0.01 39) Chrysene-dl2 39.09 240 5693969 20.00 ug/1 -0.02 45) Perylene-dl2 0.00 264 0m 20.00 ug/1 -42.31

System Monitoring Compounds 28) TCMX 26.73 207 197179 3.37 ug/1 0.17 Spiked Amount 4.000 Recovery = 84.25% 38) 2,4-DDD 0.00 235 0 0.00 ug/ml Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 04945.D SCANAPR0902.M Thu Apr 11 15:54:40 2002 Page 1

NYC-WTC_000040214

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NYC-WTC_000040214Source: NYC Law Department, mirrored locally

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