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GCMS surrogate recovery data for sample AE04945, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07634 analyzed on April 30, 2002.

NYC-WTC_000040212–000040229

Folder label: “GCMS X 4/3/02 A 4/10/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR3002\4945.D Vial: 12 Acq On : 30 Mar 2002 1:52 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 30 2:412002 ।Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.22 168 545 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 24.72 284 175 N.D. 33) Phenanthrene 25.70 178 4201 N.D. 34) Anthracene 25.70 178 4201 N.D. 35) Di-n-butylphthalate 27.60 149 18610 0.26 ug/1 # 97 36) Fluoranthene 29.33 202 4812 N.D. 39) Pyrene 30.00 202 4629 N.D. 40) Butylbenzylphthalate 32.13 149 5587 0.30 ug/1 91 41) Benzo(a)anthracene 33.64 228 9723 0.33 ug/1 96 42) Bis(2-ethylhexyl)phthalate 33.91 149 8151 0.33 ug/1 93 43) Chrysene 33.76 228 12038 0.41 ug/1 97 45) Di-n-Octylphthalate 35.65 149 4731 N.D. 46) Benzo(b)fluoranthene 36.75 252 6730 0.32 ug/1 # 87 47) Benzo(k)fluoranthene 36.82 252 8976 0.44 ug/1 # 91 48) Benzo(a)pyrene 37.74 252 3274 N.D. 49) Indeno(1,2,3-cd)pyrene 42.07 276 3372 N.D. 50) Dibenz(a,h)anthracene 42.15 278 2608 N.D. 51) Benzo(g,h,i)perylene 43.29 276 3570 N.D.

(#) = qualifier out of range (m) = manual integration 4945.D GCMS0308.M Tue Apr 02 10:56:12 2002 Page 2

NYC-WTC_000040224

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NYC-WTC_000040224Source: NYC Law Department, mirrored locally

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