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GCMS reanalysis comments for sample AE03383, April 2002

Machine-extracted title · confidence 100%

Laboratory notes indicating high recoveries and the decision to reextract and reanalyze sample AE03383 on April 16, 2002.

NYC-WTC_000040156–000040163

Folder label: “GCMS X 3/26/02 A 4/6/02

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Scanned page image, NYC-WTC_000040158
OCR text

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO 4 05\3383.D Vial: 19 Acq On 6 Apr 2002 11:39 am Operator: Sample gc/ms scan 3/26 fb Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: GOOFY.P Quant Time: Apr 15 14:29 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 15 14:10:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.69 178 799 N.D. 35) Anthracene 25.69 178 478 N.D. 36) Di-n-butylphthalate 27.61 149 1510 N.D. 37) Fluoranthene 0.00 202 0 N.D. 4 0) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.68 228 2346 N.D. 43) Bis(2-ethylhexyl)phthalate 33.90 149 1985 N.D. 44) Chrysene 33.77 228 1379 N.D. 46) Di-n-Octylphthalate 35.65 149 460 N.D. 47) Benzo(b)fluoranthene 36.76 252 693 N.D. 48) Benzo(k)fluoranthene 36.81 252 1622 N.D. 49) Benzo(a)pyrene 37.93 252 1184 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 3383.D GCMS0408.M Mon Apr 15 14:30:11 2002 Page 2

NYC-WTC_000040158

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NYC-WTC_000040158Source: NYC Law Department, mirrored locally

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