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GCMS analysis results for sample AE06991, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06991 conducted on April 16, 2002, including surrogate recovery data.

NYC-WTC_000040146–000040155

Folder label: “GCMS X 3/26/02 A 4/6/02

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Scanned page image, NYC-WTC_000040151
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APR0 4 05\6991.D Vial: 20 ’ Acq On 6 Apr 2002 1:38 pm Operator: Sample gc/ms scan 3/26 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.228 344 347 350 rBV 27641 55770 1.43% 0.322% 2 12.248 779 785 801 rVB 1038931 2669231 68.50% 15.407% 3 14.847 1062 1068 1074 rBV 155688 300004 7.70% 1.732% 4 15.884 1175 1181 1198 rBV 1638875 3400966 87.27% 19.630% 5 21.190 1752 1759 1772 rBV 1895543 3896891 100.00% 22.492%

6 23.329 1986 1992 1999 rBV 103473 208074 5.34% 1.201% 7 25.633 2236 2243 2254 rBV 1708285 3606294 92.54% 20.815% 8 33.694 3114 3121 3138 rBV2 833005 1972940 50.63% 11.388% 9 37.935 3575 3583 3599 rBV2 411632 1215173 31.18% 7.014%

Sum of corrected areas: 17325343

6991.D GCMS0408.M Mon Apr 15 14:43:39 2002

NYC-WTC_000040151

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NYC-WTC_000040151Source: NYC Law Department, mirrored locally

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