NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
‘4 Data File C:\HPCHEM\l\DATA\APR0405\6998.D Vial: 27
Acq On 6 Apr 2002 11:30 pm Operator:
Sample gc/ms scan 3/26 fb Inst : GC/MS 209
Mise Multiplr: 2.00
MS Integration Params: GOOFY.P
Quant Time: Apr 15 14:40 2002 Quant Results File: GCMS0408.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Apr 15 14:10:52 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0403
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.24 152 443974 20.00 ug/1 -0.02
10) Naphthalene-d8 15.88 136 1619535 20.00 ug/1 -0.03
17) Acenaphthene-diO 21.18 164 907250 20.00 ug/1 -0.02
30) Phenanthrene-dlO 25.63 188 1228975 20.00 ug/1 -0.03
39) Chrysene-dl 2 33.69 240 556648 20.00 ug/1 -0.03
45) Perylene-dl2 37.93 264 292029 20.00 ug/1 -0.02
System Monitoring Compounds
28) TCMX 23.32 209 29398 12.02 ug/mL 0.00
Spiked Amount 10.000 Recovery = 120.20%
38) 2,4-DDD 0.00 235 0 0.00 ug/mL
Spiked Amount 5.000 Recovery = 0.00%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.0 0 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 0.00 168 0 N.D.
32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
(#) = qualifier out of range (m) = manual integration
6998,D GCMS0408.M Mon Apr 15 14:40:51 2002 Page 1
NYC-WTC_000040081
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