GCMS analysis results for sample AE06591, April 18, 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

. Data File : C:\MSDCHEM\l\DATA\041502\6591.D Vial: 18 Acq On : 16 Apr 2002 12:02 am Operator: Bohik Sample : SAMPLE 6591 3/20/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.423 395 399 426 rBV 275790 820194 18.04% 3.436% 2 9.407 1071 1077 1098 rBV 924305 2712357 59.66% 11.363% 3 10.253 1213 1221 1230 rBV5 19085 52604 1.16% 0.220% 4 12.879 1661 1668 1690 rBV 1927451 4114371 90.50% 17.237% 5 17.985 2529 2537 2560 rBV 2182509 4546065 100.00% 19.045%

6 22.339 3269 3278 3302 rBV2 1961610 4381713 96.38% 18.357% 7 27.280 4111 4119 4138 rVB 310622 615829 13.55% 2.580% 8 30.142 4596 4606 4634 rBV2 1586469 3854918 84.80% 16.150% 9 34.014 5254 5265 5286 rBV2 1091267 2771635 60.97% 11.612%

Sum of corrected areas: 23869686

5591.D 5080402BBC.M Wed Apr 17 18:09:22 2002 Page 1

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