GCMS blank analysis for sample AE06412, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO4O5\LB. D Vial: 3 Acq On 5 Apr 2002 11:57 am Operator: Sample gc/ms scan 3/19 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 10 11:40 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 10 10:43:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 464429 20.00 ug/1 -0.02 10) Naphthalene-d8 15.88 136 1701600 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.19 164 953606 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.63 188 1335592 20.00 ug/1 -0.03 39) Chrysene-dl2 33.69 240 638674 20.00 ug/1 -0.03 45) Perylene-dl2 37.93 264 342715 20.00 ug/1 -0.02

System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery 55< 0.00% 38) 2,4-DDD 30.71 235 66957 5-44-ug/mL 0.21 Spiked Amount 5.000 Recovery = 408.80% 21’70

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.41 74 713 N.D. 3) bis(2-Chloroethyl)ether 11.52 93 211 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.48 77 190 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.94 128 591 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 20.73 152 502 N.D. 2 3) Acenaphthene 21.28 153 333 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.66 149 115 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0408.M Wed Apr 10 11:41:02 2002 Page 1

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