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GCMS analysis results for sample AE06430, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.

NYC-WTC_000039469–000039496

Folder label: “GCMS X 3/19/02 A 4/17/02

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Scanned page image, NYC-WTC_000039474
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OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 272 278 283 rBV4 10322 39082 1.09% 0.190% 2 8.099 329 333 351 rBV 179618 506816 14.14% 2.468% 3 9.953 529 535 547 rBV 9869 39226 1.09% 0.191% 4 11.615 712 716 726 rBV 19690 52921 1.48% 0.258% 5 12.212 776 781 792 rBV 1031985 2518470 70.26% 12.266%

6 14.810 1058 1064 1073 rVB 124393 235059 6.56% 1.145% 7 15.847 1171 1177 1194 rBV 1584116 3226513 90.01% 15.715% 8 17.968 1401 1408 1416 rBV 264487 503633 14.05% 2.453% 9 18.684 1481 1486 1493 rVB 76528 133625 3.73% 0.651% 10 20.805 1709 1717 1722 rBV 205706 417541 11.65% 2.034%

11 21.144 1748 1754 1765 rBV 1788612 3584515 100.00% 17.459% 12 21.557 1794 1799 1810 rVB 67669 131476 3.67% 0.640% 13 23.320 1985 1991 1997 rBV 157641 298993 8.34% 1.456% 14 25.496 2222 2228 2232 rBV 118080 232537 6.49% 1.133% 15 25.587 2232 2238 2250 rW 1622353 3314712 92.47% 16.144%

16 27.424 2433 2438 2445 rVB 83342 160353 4.47% 0.781% 17 29.186 2624 2630 2636 rBV 62752 129886 3.62% 0.633% 18 30.664 2785 2791 2796 rBV 223884 437454 12.20% 2.131% 19 30.784 2799 2804 2811 rVB 61631 127269 3.55% 0.620% 20 32.243 2957 2963 2969 rBV2 51297 111833 3.12% 0.545%

21 33.639 3105 3115 3130 rBV2 964855 2332645 65.08% 11.361% 22 34.896 3246 3252 3259 rBV2 38961 92473 2.58% 0.450% 23 36.090 3374 3382 3389 rBV 32662 80534 2.25% 0.392% 24 37.311 3508 3515 3524 rVB2 27209 84299 2.35% 0.411% 25 37.871 3568 3576 3590 rBV2 565799 1640926 45.78% 7.992%

26 38.743 3664 3671 3682 rBV3 14495 57055 1.59% 0.278% 27 40.487 3853 3861 3869 rBV4 9061 41749 1.16% 0.203%

Sum of corrected areas: 20531595

6430.D GCMS0412.M Thu Apr 18 09:09:15 2002

NYC-WTC_000039474

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NYC-WTC_000039474Source: NYC Law Department, mirrored locally

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