GCMS analysis results for sample AE06430, April 2002

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Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.

NYC-WTC_000039469–000039496

Folder label: “GCMS X 3/19/02 A 4/17/02”

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Data File : C:\HPCHEM\1\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Ethane, 1,1,2,2-tetrachloro- Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 9.95 0.31 ug/1 39226 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5 94 2 Ethane, 1,1,2-trichloro-2-fluoro- 150 C2H2C13F’ 000359-28-4 64 3 Ethane, 2,2-dichloro-1,1,1-trifluor 152 C2HC12F3 000306-83-2 59 4 Ethane, 1,2,2-trichloro-l,1-difluor 168 C2HC13F2 000354-21-2 58 Abundance Scan 535 (9.953 min): 6430.D (-) m/z 82.85 100.00% 83

5000

< ■ i < ■ > । । । < । ■ । > ' । 1 । । 47 61 95 133 166 960 9.80 10.00 10.20 - I''1''' i1 r'111 . ............................... .. .. 11 । । 11 । l , m/z 84.85 T | i i i । | i I i i । i > I I | । i i r 67.13% mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #13774: Ethane, 1,1,2,2-tetrachloro- 83

5000 TT 9.60 9.80 10.00 10.20 m/ Z 94.90 16.54% , 95 131 168 35 47 1 ‘ i.................... ' 1 TUTT 11T TH 1' ... • ■ ■ , । , ' 'II'I1 ............................ 1 1 ' ■ i ' ■ ■ 1 i ■III. ‘i‘............................ । । । । । । । । । । । । । । । |It 1 । | । । ।. । i । । । । । । । । । । 11 । । ।111 m/z-> 30 40 50 6070 80 90 100 110 120 130 140 150 160 170_ Abundance #9542: Ethane, 1,1,2-trichloro-2-fluoro- 83 .......... ;..........................

9.60 9.80 10.00 10.20 5000 m/ z 86.90 12.92% 67 95 150 0 35 47 TTTI—T TT 11 TTTTT J It _ 11 1 1 1111 > •' ' I' > < I P JI JI I J11JI I 11 ■' r 1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #66872: Ethane, 2,2-dichloro-1,1,1-trifluoro- । t ■ ■ ■ ■ । ■ 1 83 9.60 9.80 10.00 10.20 m/z 132.90 11.78% 5000 A

67 133 —35 ’ ’/2.8 1 I l ki l i ’d 1 117 i" '11'' 1 ‘ i'''' ।1 ■ *' ।11'11 11 1 111 1111 1,1 111 152 111111ii11111111 Tit m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 9.60 9.80 10.00 10.20 _

6430.D GCMS0412.M Thu Apr 18 09:09:20 2002 Page 3

NYC-WTC_000039478

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NYC-WTC_000039478Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE06449, April 2002 · Box DEP Box 23

NYC-WTC_000039497

Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.

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