GCMS analysis results for sample AE06335, April 2002

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Laboratory report documenting GCMS analysis of sample AE06335 conducted on April 18, 2002.

NYC-WTC_000039405–000039416

Folder label: “GCMS X 3/18/02 A 4/8/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020408\6335.D Vial: 19 Acq On 9 Apr 2002 3:37 am Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 09 15:20:31 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 15:05:54 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 10.66 152 4526495 20.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 17194589 20.00 ug/1 0.00 17) Acenaphthene-diO 23.67 164 10103321 20.00 ug/1 0.00 31) Phenanthrene-diO 30.91 188 16495166 20.00 ug/1 0.00 39) Chrysene-dl2 39.10 240 12686033 20.00 ug/1 -0.01 45) Perylene-dl2 42.31 264 7120331 20.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 0.00 207 0 0.00 ug/1 Spiked Amount 5.000 Recovery = 0.00% 38) 2,4-DDD 36.62 235 584482 3.17 ug/ml 0.00 Spiked Amount 5.000 Recovery = 63.40%

Target Compounds (.2-153 (21.32 Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1.3-Dichlorbenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 43 0 N.D. 9) Hexachloroethane 0.00 119 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Acenaphthylene 0.00 152 0 N.D. 21) Dimethyl phthalate 0.00 22) 2,6-Dinitrotoluene 23) Acenaphthene 24) 2,4-Dinitrotoluene 25) Fluorene 23.67 0.00 0.00 0.00 163 77 153 165 166 0 9342 0 0 0 N.D. 0.29 ug/1 # N.D. N.D. N.D. X1 26) Diethyl phthalate 0.00 149 0 N.D. 27) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 29) N-Nitrosodiphenylamine 0.00 168 0 N.D. 30) Azobenzene 0.00 77 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) 4-Bromophenyl-phenylether 0.00 248 0 N.D.

(#) = qualifier out of range (m) = manual integration 6335.D SCANAPR0902 ,M Tue Apr 09 15:21:01 2002 Page 1

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GCMS analysis results for sample AE06336, April 2002 · Box DEP Box 23

NYC-WTC_000039426

Laboratory report documenting GCMS analysis of sample AE06336 conducted on April 18, 2002.

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