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GCMS analysis results for sample AE06303, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06303 conducted on April 17, 2002.

NYC-WTC_000039332–000039341

Folder label: “GCMS X 3/18/02 A 4/8/02

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Scanned page image, NYC-WTC_000039340
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020408\6303.D Vial: 11 Acq On 8 Apr 2002 8:11 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Phenanthrene-diO Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

31.14 0.11 ug/1 289232 Phenanthrene-dl0 30.92

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 56 2 Anthracene-diO- 188 C14D10 001719-06-8 56 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 45 4 1,4-Naphthoquinone, 2,3-dihydro-... 188 C12H1202 1000157-22-3 9 Abundance Scan 4775 (31.135 min): 6303.D (-4767) (-) m/z 188.15 100.00% 188

5000

94 > • i ■ ■ ri ।1 ' ■ "III ' T । 40 80 158 30.80 31.00 31.20 31.40

m/z-> O'T ITTIT | I ' ' I [ ' I 1' I " 11111111 ‘111 m II’ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1’’ m/z 94.10 19.80% Abundance #79827: Phenanthrene-d10 188

5000 30.80 31.00 31.20 31.40 m/z 189.10 17.14% 80 94 160 O-p 30 42 52 66 TDTt i 11 । 11 11 । H h । i i H l| 108 118 I j 1111 f 11111 132 TTWTTTTTT 146—4.170179— miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 188 , TI—B—KT/m—nT j , , r-T ; , , , , | 30,80 31,00 31.20 31.40 5000 m/Z 184.10 16.48%

80 .94 160 , , 66 0- 17 TPH 30 42 52 TH....... TIut 108 118 132 146—4179179 — m/z—> 10 20 30 40 50 60 70 80 90 100 1 iC 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime ----- — ' i 188 30.80 31.00 31.20 31.40 m/ z 4 0.10 14.15%

5000 143 51 64 76 89 102 115 130 ill 158 170 o m10T ... - -----l n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 30.80 31.00 31.20 31.40

6303.D SCANAPR0902 .M Wed Apr 10 14:59:03 2002 Page 3

NYC-WTC_000039340

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NYC-WTC_000039340Source: NYC Law Department, mirrored locally

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