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GCMS calibration results for Method 508, April 2002

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Calibration report for Method 508 GC/MS analysis performed on April 10, 2002, listing internal standards.

NYC-WTC_000039315–000039319

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

User: Fakhouri, Morgan Westchester Dept. of Labs & Research Date: 04/10/2002 Time: 14:42:29

Sample: AE06303 Analysis: $REGCMS Reference for GCMS Scan Units: ug Started: 4/10/02 14:14 Ended: 4/10/02 14:14 Analyst: MF Page: 1

k n-Nitrosodimethylamine Component Name Viol [ Result MDL i

-1 3.68 2.0 12 bis(2-Chloroethyl)ether 9.29 "2.0 13 1,3-Dichlorobenzene 5.24 "2.0 4 ■ 1,4-Dichlorobenzene 5.59 "2.0 56 1,2-Dichlorobenzene 6.13 "2.0 2,2-oxybis( 1-Chloropropane) 9.02 "2.0 47 n-Nitrosodi-n-propylamine 9.71 "2.0 18 Hexachloroethane _______ 3.85 "2.0 9 : Nitrobenzene 8.40 2.0 10 ; Isophorone _______ 9.73 2.0 11 bis(2-Chloroethoxy)methane _______ 9.71________ "2.0 12 : 1,2,4-Trichlorobenzene 6.54 2.0 .13 Naphthalene _______ 8.70 2.0 14 Hexachlorobutadiene _______ 3.56________ 2.0 15 2-ChIoronaphthalene 8.00 2.0 116 Dimethylphthalate 9.69 2.0 17 2,6-Dinitrotoluene 9.18 2.0 |. 18 Acenaphthylene 8.85 2.0 7 19 Acenaphthene _______ 8.87________ 2.0 20 2,4-Dinitrotoluene 6.81 2.0 21 Diethylphthalate 9.86 2.0 22 4-Chlorophenylphenylether _____ • 8.61________ 2.0 23 Fluorene 8.98 2.0 2425 Azobenzene/1,2-Diphenylhydraz _______ 8.71_________ n-Nitrosodiphenylamine _______ 8.32________ 2.0 2.0 26 4-Bromophenylphenylether Hexa chlorobenzene 8.61 8.12 2.0 2.0 27 28 Phenanthrene 9.40 2.0 29 Anthracene _______ 8.71_________ 2.0 30 Di-n-butylphthalate _______ 10.23 ~ 2.0 “31 Fluoranthene _______ 9.10________ 2.0 32 Pyrene 10 01 2.0 33 Butylbenzylphthalate _______ 8.85 2.0 34 Benzo(a)anthracene ______ 9.57_________ 2.0 35 bis(2-Ethylhexyl)phthalate 8.73 2.0 36 Chrysene 10.14 2.0 37 Di-n-octylphthalate _______10.75________ 2.0 38 Benzo(b)fluoranthene 8.52 2.0 39 Benzo(k)fluoranthene 9.11 2.0 40 Benzo(a)pyrene ______ 6.43 2.0 41 lndeno(1,2,3-cd)pyrene ______ 10.36________ 2.0 42 Dibenz(a,h)anthracene ______ 8.67_________ 2.0 43 Benzo(g ,h, i)perylene 9.46 2.0

NYC-WTC_000039315

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NYC-WTC_000039315Source: NYC Law Department, mirrored locally

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