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GCMS analysis comments for sample AE04027, March 2002

Machine-extracted title · confidence 100%

Laboratory notes for sample AE04027 documenting low surrogate recovery and subsequent re-extraction and re-analysis on March 21, 2002.

NYC-WTC_000039183–000039189

Folder label: “GCMS X 3/14/02 A 3/17/02

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Scanned page image, NYC-WTC_000039187
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

. Data File : C:\MSDCHEM\1\DATA\031702\4027FBR.D Vial: 23 Acq On : 18 Mar 2002 4:23 am Operator: McLean Sample : 3/14/02RE EXT Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 10C Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge ICO prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.543 708 713 741 rBV 1703988 5174397 65.80% 12.579% 2 13.026 1091 1097 1113 rBV 3282161 7207151 91.64% 17.521% 3 18.133 1654 1660 1683 rBV 3935786 7864283 100.00% 19.119% 4 22.495 2135 2141 2156 rBV2 3396966 7845515 99.76% 19.073% 5 22.650 2156 2158 2169 rVB3 32126 93014 1.18% 0.226%

6 27.430 2681 2685 2695 rBV 616826 1174018 14.93% 2.854% 7 30.305 2995 3002 3022 rBV2 3252760 7343302 93.38% 17.852% 8 34.178 3422 3429 3452 rBV 1798337 4432601 56.36% 10.776%

Sum of corrected areas: 41134281

1027FBR.D 5080302.M Wed Mar 20 11:30:34 2002 Page 1

NYC-WTC_000039187

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NYC-WTC_000039187Source: NYC Law Department, mirrored locally

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