GCMS analysis comments for sample AE03915, March 2002

% Ucii L — —C — — Vi- —\M1 — ,L IS V —WSt, 0 2 2 X Data File : C:\MSDCHEM\l\DATA\031702\3915RE.D Vial: 24 K O O 3 Acq On Sample : 18 Mar 2002 : 3/14/02RE EXT 5:12 am Operator: McLean Inst : Instrumen co _s

I o Mise : Multiplr: 1.00 U o MS Integration Params: BENZO.P C o CT o Quant Time: Mar 20 11:27 2002 Quant Results File: 5080302.RES o' o C U to o Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) — Title : Quantitation For Method 508gcscan 0) 00 Last Update : Thu Mar 14 13:02:27 2002 U o Response via : Initial Calibration O C Abundance TIC: 3915RE.D 3 o — © 5000000 5 d) 5 to O s o a 4500000 8 73 £ 1 5 & N V0 s 4000000 8 z if I' th

6

3500000

$ o 3000000 § 8 N 8 8 5O 5 s 2500000 $ $ 0.

2000000

1500000 E 3 8

1000000 IN

500000 12 35 Time-> 0—= 4.00 6.00 8.00 T 1 ' 10.00 12.00 14.00 16.00 18.00 20.00 — -.......................... — 22.00I ----- 24.00 26.00 1r 28.00 30.00 32.00 -i 34.00 — i ir-iir—। 1 ir—ii r it r 36.00 38.00

3915RE.D 5080302.M Wed Mar 20 11:27:53 2002 Page 3