GCMS reference results for sample AE05902, March 2002

Quantitation Report (QT Reviewed) Z 2 - K Data File O o C:\MSDCHEM\l\DATA\031702\314REFl.D Vial: 17 3 Acq On Sample 17 Mar 2002 11:29 pm Operator: McLean Inst : Instrumen t _s

I o Mise Multiplr: 1.00 "O C o MS Integration Params: BENZO.P O o o o Quant Time: Mar 20 11:00 2002 Quant Results File: 5080302.RES o "0 C o CD O Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) — 0 Title : Quantitation For Method 508gcscan U Last Update : Thu Mar 14 13:02:27 2002 o O Response via : Initial Calibration C Abundance - TIC: 314REF1.D 3 (D

5000000

o o 4500000 y<u 00 5 d O

5 13 5 * i s» $ s ni 4000000 4 5 $ $ C)

3500000

y aa 3000000 3 o N 5O 5 N I £ 5 -8 8 P

6 $ u 3 2 ro Q o t R s5 6 0) to 2500000 3 D 8 5 59 3 E 5 £ O g8 68£ to

Jfl b I s0 s € s S 8 s5 i 6 5 e 11 I ? a 5. D 2 6 2000000 % 3 E 2 £ | a f ss ) 2 $ o s j o 8 sf 8 13 £ h s 4 h § 88 E 8 o £ g & C 56 *3 f m a s O

J2 I 1500000 8 J ! 8g 58 88 1 88 0) 8 6 Q 5 3 t E 3 2 m5 19 S.8585 N 8 1 2 s O 2 1s 1000000 S § hlHi 0 S S = N 1 (95.0 §5 5■ & 5 5 8 9 N S. 5

500000 i N 90 8 6 8 1? S CD § E S0 6 F X 5O z X

TIT f I ' P— U — ..........— r 1 T P r . 1TT , I r r 1. — . . Tlme-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 314REF1.D 5080302.M Wed Mar 20 11:02:04 2002 Page 3