GCMS quantitative results for sample AE02092, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) • ‘Data File C:\MSDCHEM\1\DATA\0 318 0 2\REFA2.D Vial: 18 Acq On 19 Mar 2002 4:05 pm Operator: McLean Sample GC/MS SCAN 3/8 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 20 02:46:00 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.54 150 1407798 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 3672470 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.13 164 2026115 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.50 188 3143307 20.00 ug/L 0.00 38) Chrysene-dl2 3 0.31 240 2972667 20.00 ug/L 0.00 44) Perylene-dl2 34.18 264 1636095 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.44 235 229186 6.11 ug/L 0.00 Spiked Amount 5.000 Recovery = 122.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.61 74 116436 3.68 ug/L 100 3) bis(2-chloroethyl) ether 8.98 93 402572 8.08 ug/L 84 4) 1,3 - Dichlorobenze 9.38 146 206319 4.19 ug/L 97 5) 1,4 - Dichlorobenzene 9.59 146 228713 4.65 ug/L 95 6) 1,2 - Dichlorobenzene 9.97 146 260115 5.72 ug/L 97 7) 2,2 ‘ - oxybis (l-Chloropr 10.43 45 1001712 8.82 ug/L 99 8) N-Nitroso-di-n-propylamine 10.75 70 357194 9.97 ug/L 99 9) Hexachloroethane 10.86 117 47461 2.57 ug/L 92 11) Nitrobenzene 11.10 77 398288 6.02 ug/L 95 12) Isophorone 11.81 82 1045295 8.59 ug/L 99 13) bis(2-Chloroethoxy) methan 12.55 93 522189 7.13 ug/L 99 14) 1,2,4-Trichlorobenzene 12.90 180 216428 5.15 ug/L 98 15) Naphthalene 13.08 128 1103319 7.23 ug/L 99 16) Hexachlorobutadiene 13.53 225 33015 1.40 ug/L 98 18) Hexachlorocyclopentadiene 15.61 237 7926 0.44 ug/L 87 19) 2-chloronaphthalene 16.51 162 544856 5.89 ug/L 98 20) Dimethylphthalate 17.59 163 976246 8.84 ug/L 99 21) 2,6-Dinitrotoluene 17.70 165 168939 7.19 ug/L 99 22) Acenaphthylene 17.69 152 1074124 8.37 ug/L 98 23) Acenaphthene 18.22 153 704032 8.07 ug/L 98 24) 2,4-Dinitrotoluene 16.85 165 216098 6.42 ug/L 99 25) Diethylphthalate 19.72 149 962295 10.13 ug/L 100 26) 4-Chlorophenyl-phenyl ethe 19.89 204 399226 7.88 ug/L 97 27) Fluorene 19.76 166 921218 8.96 ug/L 100 28) Azobenzen/ 1,2-Diphenylhyd 20.34 77 1132072 8.08 ug/L 98 30) N-Nitrosodiphenylamine 20.26 169 550825 8.15 ug/L 99 31) 4-Bromophenyl-phenyl ether 21.32 248 236543 8.52 ug/L 97 32) Hexachlorobenzene 21.34 284 230110 7.86 ug/L 96 33) Phenanthrene 22.56 178 1344155 9.23 ug/L 99 34) Anthracene 22.70 178 1272562 8.81 ug/L 100 35) Di-n-butylphthalate 24.65 149 1635468 9.80 ug/L 99 36) Fluoranthene 26.06 202 1563593 9.45 ug/L 99 39) Pyrene 26.69 202 1675760 8.15 ug/L 97 40) Butylbenzylphthalate 29.05 149 673444 7.65 ug/L 99 41) Benzo (a) antracene 30.29 228 1290801 8.27 ug/L 98 42) Bis (2-ethylhexyl) phthala 30.91 149 915291 7.87 ug/L 98 43) Chrysene 3 0.38 228 1435998 9.69 ug/L 98 45) Di-n-Octylphthalate 32.75 149 1236429 7.04 ug/L 98 46) Benzo (b) fluoranthene 33.23 252 1037260 9.00 ug/L 99

(#) = qualifier out of range (m) = manual integration REFA2.D 5080302.M Wed Mar 20 02:46:05 2002 Page 1

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